Registration Dossier
Registration Dossier
Please be aware that this old REACH registration data factsheet is no longer maintained; it remains frozen as of 19th May 2023.
The new ECHA CHEM database has been released by ECHA, and it now contains all REACH registration data. There are more details on the transition of ECHA's published data to ECHA CHEM here.
Use of this information is subject to copyright laws and may require the permission of the owner of the information, as described in the ECHA Legal Notice.
EC number: 813-399-9 | CAS number: 1821694-26-1
Melting point / freezing point
Administrative data
Link to relevant study record(s)
- Endpoint:
- melting point/freezing point
- Type of information:
- experimental study
- Adequacy of study:
- key study
- Study period:
- 2015
- Reliability:
- 2 (reliable with restrictions)
- Rationale for reliability incl. deficiencies:
- study well documented, meets generally accepted scientific principles, acceptable for assessment
- Qualifier:
- according to guideline
- Guideline:
- other: ISO 11357-3:2011
- Version / remarks:
- DSC Method : Plastics-differential scanning calorimetry (DSC). Part 3 :Determination of temperature enthalphy of melting and crystallization
Standard : ISO 11357-3 :2011 - Deviations:
- not specified
- Principles of method if other than guideline:
- DSC: Plastics-differential scanning calorimetry (DSC).
Equipment: TA Instruments DSC Q20, no EQ661
Temperature program: 20-320°C at 20°C/min.
Sample holders: Crucible of aluminium
Sample size: 9 ± 1 mg.
Atmosphere: Nitrogen
Ambient temperature: 23ºC
Relative humidity: 50% - GLP compliance:
- no
- Other quality assurance:
- other: not specified
- Type of method:
- thermal analysis
- Remarks:
- additionally, the sample was analysed by capillary tube method.
- Specific details on test material used for the study:
- SOURCE OF TEST MATERIAL
- Source and lot/batch No.of test material: Lot Nr. 4145Z0514
- Purity test date: 2015-11-26 - Key result
- Decomposition:
- yes
- Decomp. temp.:
- 130 °C
- Remarks on result:
- other:
- Remarks:
- Glass transition temperature is 68.34 °C
- Conclusions:
- Based on results in this report: The substance decomposes before melting at 130ºC.
- Executive summary:
Melting point of Magnesium glucoheptonate was analysed by plastics-differential scanning calorimetry (DSC) (Part 3 :Determination of temperature enthalphy of melting and crystallization according to standard method: ISO 11357-3 : 2011). Since the DSC melting curve had the tipical profile from a decomposition without melting, the sample was analized also by the technique Capillary tube melting point to corroborate this results by visual observation. A decomposition before melting have also been observed.
In conclusion, according to DSC methof glas transition temperature is 68.34 °C. Overall conclusion: the substance decomposes before melting at 130ºC.
Reference
Description of key information
The substance decomposes before melting at 130ºC.
Key value for chemical safety assessment
Additional information
Information on Registered Substances comes from registration dossiers which have been assigned a registration number. The assignment of a registration number does however not guarantee that the information in the dossier is correct or that the dossier is compliant with Regulation (EC) No 1907/2006 (the REACH Regulation). This information has not been reviewed or verified by the Agency or any other authority. The content is subject to change without prior notice.
Reproduction or further distribution of this information may be subject to copyright protection. Use of the information without obtaining the permission from the owner(s) of the respective information might violate the rights of the owner.
