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Please be aware that this old REACH registration data factsheet is no longer maintained; it remains frozen as of 19th May 2023.

The new ECHA CHEM database has been released by ECHA, and it now contains all REACH registration data. There are more details on the transition of ECHA's published data to ECHA CHEM here.

Diss Factsheets

Physical & Chemical properties

Melting point / freezing point

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Administrative data

Link to relevant study record(s)

Reference
Endpoint:
melting point/freezing point
Type of information:
experimental study
Adequacy of study:
key study
Study period:
2021
Reliability:
1 (reliable without restriction)
Rationale for reliability incl. deficiencies:
guideline study
Qualifier:
according to guideline
Guideline:
OECD Guideline 102 (Melting point / Melting Range)
Version / remarks:
1995
Deviations:
no
GLP compliance:
no
Type of method:
method to determine freezing temperature
Key result
Melting / freezing pt.:
< -30 °C
Decomposition:
no
Sublimation:
no
Remarks on result:
other: The test item did not freeze during the test. Therefore, no exact freezing temperature can be reported.
Conclusions:
The freezing point of the test item was determined to be below -30 °C (253 K).
Executive summary:

An experimental study was conducted according to OECD Test Guidelines 102 to determine the freezing point of the test item. The test was performed using a sample flask with a screw lid to support a thermometer. For agitating a magnetic bar stirrer was placed into the sample flask. The sample flask is cooled down in a dry ice / acetone bath to -30 °C for a period of 1 h. The test was performed in duplicate. The test item did not freeze during the test. Therefore, no exact freezing temperature can be reported. The freezing point of the test item was determined to be below -30 °C (253 K).

Description of key information

The freezing point of the test item was determined to be below -30 °C (253 K).

Key value for chemical safety assessment

Additional information

An experimental study was conducted according to OECD Test Guidelines 102 to determine the freezing point of the test item. The test was performed using a sample flask with a screw lid to support a thermometer. For agitating a magnetic bar stirrer was placed into the sample flask. The sample flask is cooled down in a dry ice / acetone bath to -30 °C for a period of 1 h. The test was performed in duplicate. The test item did not freeze during the test. Therefore, no exact freezing temperature can be reported. The freezing point of the test item was determined to be below -30 °C (253 K).