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Reaction product of 3-[4-(2-aminoethylamino)-6-(4-sulfoanilino)-1,3,5-heterocycle-2-ylamino]benzensulfonic acid, ammonia water, sodium chloride and {mixture of [poly(1~4)chlorosulfonylphthalocyaninato-N29,N30,N31,N32]copper(II), [poly(1~3)chlorosulfonyl (tribenzo[b,g,l]pyrido[2,3-q]-5,10,15,20-tetraazaporphyrinato-N21,N22,N23,N24)]copper(II),[poly(1~2)chlorosulfonyl(dibenzol[b,g(or b,l)dipyrido[2,3(or 3,2)-l,q (or g,q)]-5,10,15,20-tetraazaporphyrinato-N21,N22,N23,N24)] copper(II) and [monochlorosulfonyl(benzo[b]tripyridol[2,3(or 3,2)-g,lq]-5,10,15,20- tetraazaporphyrinato- N21,N22,N23,N24)] copper(II)
EC number: - | CAS number: -
- Life Cycle description
- Uses advised against
- Endpoint summary
- Appearance / physical state / colour
- Melting point / freezing point
- Boiling point
- Density
- Particle size distribution (Granulometry)
- Vapour pressure
- Partition coefficient
- Water solubility
- Solubility in organic solvents / fat solubility
- Surface tension
- Flash point
- Auto flammability
- Flammability
- Explosiveness
- Oxidising properties
- Oxidation reduction potential
- Stability in organic solvents and identity of relevant degradation products
- Storage stability and reactivity towards container material
- Stability: thermal, sunlight, metals
- pH
- Dissociation constant
- Viscosity
- Additional physico-chemical information
- Additional physico-chemical properties of nanomaterials
- Nanomaterial agglomeration / aggregation
- Nanomaterial crystalline phase
- Nanomaterial crystallite and grain size
- Nanomaterial aspect ratio / shape
- Nanomaterial specific surface area
- Nanomaterial Zeta potential
- Nanomaterial surface chemistry
- Nanomaterial dustiness
- Nanomaterial porosity
- Nanomaterial pour density
- Nanomaterial photocatalytic activity
- Nanomaterial radical formation potential
- Nanomaterial catalytic activity
- Endpoint summary
- Stability
- Biodegradation
- Bioaccumulation
- Transport and distribution
- Environmental data
- Additional information on environmental fate and behaviour
- Ecotoxicological Summary
- Aquatic toxicity
- Endpoint summary
- Short-term toxicity to fish
- Long-term toxicity to fish
- Short-term toxicity to aquatic invertebrates
- Long-term toxicity to aquatic invertebrates
- Toxicity to aquatic algae and cyanobacteria
- Toxicity to aquatic plants other than algae
- Toxicity to microorganisms
- Endocrine disrupter testing in aquatic vertebrates – in vivo
- Toxicity to other aquatic organisms
- Sediment toxicity
- Terrestrial toxicity
- Biological effects monitoring
- Biotransformation and kinetics
- Additional ecotoxological information
- Toxicological Summary
- Toxicokinetics, metabolism and distribution
- Acute Toxicity
- Irritation / corrosion
- Sensitisation
- Repeated dose toxicity
- Genetic toxicity
- Carcinogenicity
- Toxicity to reproduction
- Specific investigations
- Exposure related observations in humans
- Toxic effects on livestock and pets
- Additional toxicological data
Water solubility
Administrative data
- Endpoint:
- water solubility
- Type of information:
- experimental study
- Adequacy of study:
- key study
- Study period:
- 08 January 2009 to 07 February 2009
- Reliability:
- 1 (reliable without restriction)
- Rationale for reliability incl. deficiencies:
- other: Study conducted in compliance with agreed protocols, with no or minor deviations from standard test guidelines and/or minor methodological deficiencies, which do not affect the quality of relevant results.
Data source
Reference
- Reference Type:
- study report
- Title:
- Unnamed
- Year:
- 2 009
- Report date:
- 2009
Materials and methods
Test guideline
- Qualifier:
- according to guideline
- Guideline:
- EU Method A.6 (Water Solubility)
- Deviations:
- not specified
- GLP compliance:
- yes (incl. QA statement)
- Remarks:
- Date of inspection: 19 August 2008; Date of signature: 04 March 2009
- Type of method:
- flask method
Test material
Reference
- Name:
- Unnamed
- Type:
- Constituent
- Details on test material:
- Sponsor's identification : H-CB sodium salt
Description : blue solid
Purity : 94.8%
Lot number : MB-2
Date received : 04 December 2008
Storage conditions : room temperature in the dark
Results and discussion
Water solubility
- Water solubility:
- 31.6 - 34 other: % w/w
- Temp.:
- 20 °C
- pH:
- > 7.6 - < 7.7
Any other information on results incl. tables
Preliminary test
The sample concentration, observations and solution pH, on completion of the 20oC equilibration period, are shown in the following table:
Sample Number |
Concentration (% w/w) |
Observations |
Solution pH |
1 |
10.1 |
Dark blue solution with no visible excess test material |
7.4 |
2 |
20.0 |
Dark blue solution with excess test material |
7.8 |
3 |
29.9 |
Dark blue viscous solution with no visible excess test material |
7.3 |
4 |
39.7 |
Dark blue very viscous solution with excess test material |
- |
5 |
49.1 |
Dark blue very viscous solution with excess test material |
- |
6 |
59.8 |
No solution present but damp test material |
- |
Result: Solubility in the range 29.9 to 39.7% w/w of solution at 20oC +/- 0.5oC.
Definitive test
The sample concentration, observations and solution pH, on completion of the 20oC equilibration period, are shown in the following table:
Sample Number |
Concentration (% w/w) |
Observations |
Solution pH |
1 |
29.7 |
Dark blue viscous solution with no visible excess test material |
7.7 |
2 |
31.6 |
Dark blue viscous solution with no visible excess test material |
7.6 |
3 |
34.0 |
Dark blue immobile paste, no visible excess test material |
- |
4 |
35.1 |
Dark blue immobile paste, no visible excess test material |
- |
5 |
37.8 |
Dark blue immobile paste, no visible excess test material |
- |
6 |
40.0 |
Dark blue immobile paste, no visible excess test material |
- |
Result: Solubility in the range 31.6 to 34.0% w/w of solution at 20oC +/- 0.5oC.
Discussion
The EC A6 Method and OECD Method 105 were not applicable due to extremely high water solubility of the test material. It was therefore not possible to prepare samples at five times saturation level as specified in the guidelines. Therefore a number of individual samples were prepared at increasing nominal concentrations and the solubility determined by visual assessment of the resulting solutions.
Although no excess test material was visible for Samples 3 to 6 in the definitive test, they formed an immobile paste which did not move or pour when held horizontally. The solubility range was therefore taken between the highest mobile concentration and the lowest stationary concentration.
Applicant's summary and conclusion
- Conclusions:
- Interpretation of results (migrated information): very soluble (> 10000 mg/L)
The water solubility of the test material has been determined to be in the range 31.6 to 34.0% w/w of solution at 20 Deg C +/- 0.5 Deg C by visual assessment. - Executive summary:
In the range 31.6 to 34.0% w/w of solution at 20oC +/- 0.5oC, based on the flask method, Method A6 Water Solubility of Commission Regulation (EC) No 440/2008 of 30 May 2008.
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