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Diss Factsheets

Physical & Chemical properties

Particle size distribution (Granulometry)

Administrative data

Endpoint:
particle size distribution (granulometry)
Type of information:
experimental study
Adequacy of study:
key study
Study period:
October 2009
Reliability:
2 (reliable with restrictions)
Rationale for reliability incl. deficiencies:
other: Study performed according to Clariant internal standard operating procedure for particle size determination

Data source

Reference
Reference Type:
study report
Title:
Unnamed
Year:
2009
Report date:
2009

Materials and methods

Test guideline
Qualifier:
no guideline required
Principles of method if other than guideline:
Laboratory test was carried out with a Malvern Mastersizer 2000.
Determination of particle size distribution in dried condition with Sirocco 2000(A) accessory.
GLP compliance:
no
Type of method:
Laser scattering/diffraction
Type of distribution:
volumetric distribution

Test material

Constituent 1
Reference substance name:
NMSBA
IUPAC Name:
NMSBA
Constituent 2
Chemical structure
Reference substance name:
4-methanesulfonyl-2-nitrobenzoic acid
EC Number:
601-017-1
Cas Number:
110964-79-9
Molecular formula:
C8 H7 N1 O6 S1
IUPAC Name:
4-methanesulfonyl-2-nitrobenzoic acid
Details on test material:
Study performed on Commercial Batch n°30014009 which relates to NMSBA crude containing 15% water but in line with substance identity as described in Section 1.2; Due to the sticky behaviour, before analysis, the crude wet product has to be dried in oven at 120°C during 48 hours.

Results and discussion

Particle sizeopen allclose all
Percentile:
D50
Remarks on result:
other: Migrated from fields under 'Mass median diameter' as D50 percentile. No source field for Standard deviation.
Percentile:
D10
Mean:
43 µm
Remarks on result:
other: 3 trials have been done but no standard deviation figure available
Percentile:
D50
Mean:
122 µm
Remarks on result:
other: 3 trials have been done but no standard deviation figure available
Percentile:
D90
Mean:
390 µm
Remarks on result:
other: 3 trials have been done but no standard deviation figure available

Applicant's summary and conclusion

Conclusions:
The particule size distribution has been performed and results are as follow: d(0.1) :43µm; d(0.5) :122µm; d(0.9) :390µm
Executive summary:

The particule size distribution has been performed and results are as follow: d(0.1) :43µm; d(0.5) :122µm; d(0.9) :390µm