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Physical & Chemical properties

Particle size distribution (Granulometry)

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Reference
Endpoint:
particle size distribution (granulometry)
Type of information:
experimental study
Adequacy of study:
key study
Study period:
6/5/2016-6/5/2016
Reliability:
1 (reliable without restriction)
Rationale for reliability incl. deficiencies:
guideline study
Justification for type of information:
Experimental test result performed using standard test guidelines
Qualifier:
according to guideline
Guideline:
other: granulometric analysis with rotap sieve shaker.
Principles of method if other than guideline:
The particle size distribution of test item3,4,5,6-tetrachloro-2-(1,4,5,8-tetrabromo-6-hydroxy-3-oxoxanthen-9-yl)benzoic acid(CAS No. 18472-87-2) was determined by granulometric analysis with rotap sieve shaker.
GLP compliance:
no
Type of method:
sieving
Type of particle tested:
primary particle
Type of distribution:
counted distribution
Percentile:
D50
Remarks on result:
other: Mass median diameter
No.:
#1
Size:
150 µm
Distribution:
21 %
No.:
#2
Size:
106 µm
Distribution:
29 %
No.:
#3
Size:
75 µm
Distribution:
29.6 %
No.:
#4
Size:
53 µm
Distribution:
18.67 %
No.:
#5
Size:
25 µm
Distribution:
0.23 %

OBSERVATION TABLE:

Amount of test item weighed (g) =10 g

Method run time (min) =10 min

Sieve sizes(in microns)

Weight of petridishes (g)

Weight of petridishes +

test item (g)

Test item quantity retained after sieving (g)

Percentage (%) of test item*

150 microns

47.147

49.247

2.100

21%

106 microns

49.512

52.412

2.900

29%

75 microns

41.219

44.179

2.960

29.60 %

53 microns

48.347

50.214

1.867

18.67 %

25 microns

37.791

37.814

0.023

0.23 %

10 microns

39.231

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*Percentage of test item=       test item retained after sievingX 100

                                                               Original test item taken

Conclusions:
The particle size distribution of test substance was determined by Granulometric analysis with Rotap sieve shaker. The particle size distribution was determined to be in the range of 150 micron to 25 micron.
Executive summary:

The particle size distribution of test substance  was determined by Granulometric analysis with Rotap sieve shaker. The particle size distribution was determined to be in the range of 150 micron to 25 micron.

Description of key information

The particle size distribution of test substance  was determined by Granulometric analysis with Rotap sieve shaker. The particle size distribution was determined to be in the range of 150 micron to 25 micron.

Additional information

The particle size distribution of test substance  was determined by Granulometric analysis with Rotap sieve shaker. The particle size distribution was determined to be in the range of 150 micron to 25 micron.