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Please be aware that this old REACH registration data factsheet is no longer maintained; it remains frozen as of 19th May 2023.

The new ECHA CHEM database has been released by ECHA, and it now contains all REACH registration data. There are more details on the transition of ECHA's published data to ECHA CHEM here.

Diss Factsheets

Administrative data

Endpoint:
melting point/freezing point
Type of information:
experimental study
Adequacy of study:
key study
Study period:
02 March 2015-19 June 2015
Reliability:
1 (reliable without restriction)
Rationale for reliability incl. deficiencies:
other: GLP-compliant study in accordance with EC A.1, OECD 102 and EPA OPPTS 830.7200.
Cross-reference
Reason / purpose for cross-reference:
reference to same study

Data source

Reference
Reference Type:
study report
Title:
Unnamed
Year:
2015
Report date:
2015

Materials and methods

Test guidelineopen allclose all
Qualifier:
according to guideline
Guideline:
EU Method A.1 (Melting / Freezing Temperature)
Version / remarks:
(2008)
Deviations:
no
Qualifier:
according to guideline
Guideline:
OECD Guideline 102 (Melting point / Melting Range)
Version / remarks:
(1995)
Deviations:
no
Qualifier:
according to guideline
Guideline:
EPA OPPTS 830.7200 (Melting Point / Melting Range)
Version / remarks:
(1998)
Deviations:
no
GLP compliance:
yes
Type of method:
thermal analysis
Remarks:
(differential scanning calorimetry)

Test material

Constituent 1
Chemical structure
Reference substance name:
3-[3-(1,1,1,3,5,5,5-heptamethyltrisiloxan-3-yl)propoxy]propane-1,2-diol
EC Number:
807-413-2
Cas Number:
70280-68-1
Molecular formula:
C13H34O5Si3
IUPAC Name:
3-[3-(1,1,1,3,5,5,5-heptamethyltrisiloxan-3-yl)propoxy]propane-1,2-diol
Test material form:
other: liquid
Details on test material:
- Name (as cited in study report): X-22-1927
- Appearance: clear light yellow liquid
- Storage conditions: at room temperature

Results and discussion

Melting / freezing pointopen allclose all
Melting / freezing pt.:
< -90 °C
Remarks on result:
other: Result from DSC Experiment 1.
Melting / freezing pt.:
< -80 °C
Remarks on result:
other: Result from 'Storage experiment in freezers'.

Any other information on results incl. tables

The test substance was observed to be a viscous liquid after storage at -21.8 ± 0.3°C and a very viscous liquid after storage at -81.6 ± 1.8°C.

Applicant's summary and conclusion

Conclusions:
The freezing temperature of X-22-1927 is < -80°C.