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Please be aware that this old REACH registration data factsheet is no longer maintained; it remains frozen as of 19th May 2023.

The new ECHA CHEM database has been released by ECHA, and it now contains all REACH registration data. There are more details on the transition of ECHA's published data to ECHA CHEM here.

Diss Factsheets

Administrative data

Endpoint:
melting point/freezing point
Type of information:
experimental study
Adequacy of study:
key study
Study period:
15 February 2018
Reliability:
1 (reliable without restriction)
Rationale for reliability incl. deficiencies:
guideline study

Data source

Reference
Reference Type:
study report
Title:
Unnamed
Year:
2018
Report date:
2018

Materials and methods

Test guidelineopen allclose all
Qualifier:
according to guideline
Guideline:
EU Method A.1 (Melting / Freezing Temperature)
Deviations:
no
Qualifier:
according to guideline
Guideline:
OECD Guideline 102 (Melting point / Melting Range)
Deviations:
no
GLP compliance:
yes (incl. QA statement)
Type of method:
method to determine freezing temperature

Test material

Constituent 1
Chemical structure
Reference substance name:
3-morpholinopropylamine
EC Number:
204-590-2
EC Name:
3-morpholinopropylamine
Cas Number:
123-00-2
Molecular formula:
C7H16N2O
IUPAC Name:
3-morpholin-4-ylpropan-1-amine
Test material form:
liquid
Specific details on test material used for the study:
SOURCE OF TEST MATERIAL
- Source and lot/batch No.of test material: 7E401

STABILITY AND STORAGE CONDITIONS OF TEST MATERIAL
- Storage condition of test material: At room temperature, at 20 ± 5 °C
- Description: Clear and substantially free of foreign matter
- Purity: 99.8 %
- Expiration Date: November 11, 2018

Results and discussion

Melting / freezing point
Key result
Melting / freezing pt.:
< -20 °C
Decomposition:
no
Sublimation:
no
Remarks on result:
other: No atmospheric pressure was recorded for this endpoint.

Any other information on results incl. tables

The mean of at least two measurements, which are in the range of the estimated accuracy of ± 0.5°C, is reported as the freezing temperature/range.

The temperature range of the equipment is -20°C to 150°C.

During screening run, 10.3g of sample was held at -25°C for approximately 10 hours. However no crystallisation was observed. As a result no further testing was performed.

Applicant's summary and conclusion

Conclusions:
The freezing point of the test item was determined to be < -20°C.