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Physical & Chemical properties

Particle size distribution (Granulometry)

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Reference
Endpoint:
particle size distribution (granulometry)
Type of information:
experimental study
Adequacy of study:
key study
Study period:
December 07th, 2017
Reliability:
1 (reliable without restriction)
Rationale for reliability incl. deficiencies:
test procedure in accordance with generally accepted scientific standards and described in sufficient detail
Qualifier:
according to guideline
Guideline:
OECD Guideline 110 (Particle Size Distribution / Fibre Length and Diameter Distributions - Method A: Particle Size Distribution (effective hydrodynamic radius)
Version / remarks:
1981
Qualifier:
according to guideline
Guideline:
ISO 13320 (Particle size analysis - Laser diffraction methods)
Version / remarks:
2009
Qualifier:
according to guideline
Guideline:
other: CIPAC MT 187 (Particle Size Analysis by Laser Diffraction)
Version / remarks:
2009
GLP compliance:
no
Type of method:
Laser scattering/diffraction
Type of particle tested:
primary particle
Type of distribution:
volumetric distribution
Percentile:
D10
Mean:
7.9 µm
St. dev.:
0.21
Percentile:
D50
Mean:
35.8 µm
St. dev.:
0.57
Percentile:
D90
Mean:
97.2 µm
St. dev.:
1.77

Particle size (µm)
D10 D50 D90
Test series 1 8.1 36.2 98.4
Test series 2 7.8 35.4 95.9

Average

7.9 35.8 97.2

SD

0.21 0.57 1.77
Conclusions:
D50: 35.8 ± 0.57 µm
Executive summary:

The particle size distribution was determined using laser diffraction. As measuring device, a Malvern Mastersizer 2000 was used. The powder was brought via a powder dispersing cell Scirocco 2000 into the laser light beam and the diffraction pattern was determined. From the diffraction pattern the particle size distribution was calculated.

Two test series of 3 measurements each were performed with test item.

The average D10 resulted to be 7.9 µm; D50 resulted to be 35.8 µm; D90 resulted to be 97.2 µm.

Conclusion

D50: 35.8 ± 0.57 µm

Description of key information

D50: 35.8 ± 0.57 µm

Additional information

ISO 13320 - Laser scattering/diffraction