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Diss Factsheets

Physical & Chemical properties

Boiling point

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Administrative data

Link to relevant study record(s)

Reference
Endpoint:
boiling point
Type of information:
experimental study
Adequacy of study:
key study
Study period:
2017-11-10 to 2018-03-20
Reliability:
1 (reliable without restriction)
Rationale for reliability incl. deficiencies:
guideline study
Qualifier:
according to guideline
Guideline:
EU Method A.2 (Boiling Temperature)
Deviations:
no
Qualifier:
according to guideline
Guideline:
OECD Guideline 103 (Boiling Point)
Deviations:
no
GLP compliance:
yes (incl. QA statement)
Type of method:
differential scanning calorimetry
Specific details on test material used for the study:
- Batch No.of test material: PFW110370
- Purity: 99.1%
- Expiration date of the lot/batch: 31 December 2018
- Storage conditions: Room temperature, in the dark
Key result
Decomposition:
yes
Decomp. temp.:
ca. 174 °C
Remarks on result:
other: No boiling observed below the temperature of decomposition

Thermographic Data

 

 

Thermal Event

 

 

Interpretation

Temperature

Det. 1

Det. 2

Det. 3

Det. 4

ºC

°C

ºC

K

Exotherm

Decomposition left limit

174.20

177.52

182.49

188.90

Endotherm

Further decomposition left limit

295.02

294.41

-

-

 

 

Thermal Event

 

 

Interpretation

Temperature

Det. 5

Det. 6

ºC

ºC

Exotherm

Decomposition left limit

184.35

182.68

Endotherm

Further decomposition left limit

302.80

301.52

Atmospheric pressure:           

Determinations 1, 2, 5 and 6: 101.6 kPa

Determinations 3 and 4: 99.0 kPa

The test item decomposed from approximately 174 °C (447 K)

Conclusions:
The test item was determined to decompose from approximately 174 °C (447 K) at 99.0 to 101.6 kPa. As the test item decomposed, no value for boiling point could be determined.

Description of key information

A GLP study was performed according to OECD guideline 103 and EU Method A.2. The test item was determined to decompose from approximately 174 °C (447 K) at 99.0 to 101.6 kPa. As the test item decomposed, no value for boiling point could be determined (K1, Envigo, 2018).

Key value for chemical safety assessment

Additional information

As the test item decomposed, no value for boiling point could be determined.