Registration Dossier
Registration Dossier
Please be aware that this old REACH registration data factsheet is no longer maintained; it remains frozen as of 19th May 2023.
The new ECHA CHEM database has been released by ECHA, and it now contains all REACH registration data. There are more details on the transition of ECHA's published data to ECHA CHEM here.
Use of this information is subject to copyright laws and may require the permission of the owner of the information, as described in the ECHA Legal Notice.
EC number: 445-910-2 | CAS number: 1388152-30-4
Melting point / freezing point
Administrative data
- Endpoint:
- melting point/freezing point
- Type of information:
- experimental study
- Adequacy of study:
- key study
- Study period:
- 04 june 2003 - 04 July 2003
- Reliability:
- 1 (reliable without restriction)
- Rationale for reliability incl. deficiencies:
- other: Study conducted in 2003 according to ASTM E537-86, Method A1 of the Commission Directive 92/69/EEC and in accordance with GLP. Study material is well characterized.
Data source
Reference
- Reference Type:
- study report
- Title:
- Unnamed
- Year:
- 2 003
- Report date:
- 2003
Materials and methods
Test guideline
- Qualifier:
- according to guideline
- Guideline:
- EU Method A.1 (Melting / Freezing Temperature)
- Version / remarks:
- Commission Directive 92/69/EEC, A1 (differential scanning calorimetry method).
- Deviations:
- no
- GLP compliance:
- yes
- Type of method:
- thermal analysis
- Remarks:
- Differential Scanning Calorimetry
Test material
- Reference substance name:
- -
- EC Number:
- 445-910-2
- EC Name:
- -
- Cas Number:
- 1388152-30-4
- Molecular formula:
- Hill formula: C24 H32 N2 O7 Si CAS formula: C15 H20 O3 Si . C9 H12 N2 O4
- IUPAC Name:
- (1R,2R)-1,3-Dihydroxy-1-(4-nitrophenyl)propyl-2-ammonium (1R, 5S)-5-(dimethylphenylsilyl)-2-(hydroxymethyl)cyclopent-2-ene-1-carboxylate
Constituent 1
Results and discussion
Melting / freezing point
- Melting / freezing pt.:
- >= 407 - <= 424 K
- Atm. press.:
- ca. 101.3 kPa
- Remarks on result:
- other: Measured at atmospheric pressure
Any other information on results incl. tables
Determination #1
| Thermal event | Interpretation | Temperature | |
| oC | K | ||
| Endotherm | Lossof volatiles/water | 105.1 | 378 |
| Double endotherm | Melting range | 134.1 - 151.2 | 407 - 424 |
Determination #2
| Thermal event | Interpretation | Temperature | |
| oC | K | ||
| Endotherm | Lossof volatiles/water | 105.9 | 379 |
| Double endotherm | Melting range | 133.7 - 151.0 | 407 - 424 |
Applicant's summary and conclusion
- Conclusions:
- The melting/freezing temperature of the test material has been determined to be 407 to 424 +/- 0.5 K
- Executive summary:
The melting/freezing temperature of the test material has been determined by DSC to be 407 to 424 +/- 0.5 K
Information on Registered Substances comes from registration dossiers which have been assigned a registration number. The assignment of a registration number does however not guarantee that the information in the dossier is correct or that the dossier is compliant with Regulation (EC) No 1907/2006 (the REACH Regulation). This information has not been reviewed or verified by the Agency or any other authority. The content is subject to change without prior notice.
Reproduction or further distribution of this information may be subject to copyright protection. Use of the information without obtaining the permission from the owner(s) of the respective information might violate the rights of the owner.
