Registration Dossier
Registration Dossier
Please be aware that this old REACH registration data factsheet is no longer maintained; it remains frozen as of 19th May 2023.
The new ECHA CHEM database has been released by ECHA, and it now contains all REACH registration data. There are more details on the transition of ECHA's published data to ECHA CHEM here.
Use of this information is subject to copyright laws and may require the permission of the owner of the information, as described in the ECHA Legal Notice.
EC number: 810-766-5 | CAS number: 1802886-42-5
Melting point / freezing point
Administrative data
Link to relevant study record(s)
- Endpoint:
- melting point/freezing point
- Type of information:
- experimental study
- Adequacy of study:
- supporting study
- Study period:
- from 2017-05-22 to 2017-11-14
- Reliability:
- 1 (reliable without restriction)
- Rationale for reliability incl. deficiencies:
- guideline study
- Qualifier:
- according to guideline
- Guideline:
- OECD Guideline 102 (Melting point / Melting Range)
- Deviations:
- no
- Qualifier:
- according to guideline
- Guideline:
- EU Method A.1 (Melting / Freezing Temperature)
- Deviations:
- no
- Qualifier:
- according to guideline
- Guideline:
- EPA OPPTS 830.7200 (Melting Point / Melting Range)
- Deviations:
- no
- GLP compliance:
- yes (incl. QA statement)
- Type of method:
- differential scanning calorimetry
- Key result
- Melting / freezing pt.:
- -25 °C
- Decomposition:
- no
- Sublimation:
- no
- Conclusions:
- The freezing point of the test item was determined with DSC to be -25 °C.
- Executive summary:
A study was conducted according to OECD TG 102, Regulation (EC) No 440/2008 method A.1 and EPA OPPTS 830.7200 to determine the freezing point of the test item using differential scanning calorimetry. The test item was weighed into an aluminium crucible under an inert atmosphere (nitrogen). Three tests were performed. As reference crucible, an empty aluminium crucible was used. The substance is a liquid at ambient conditions. Therefore, the crucibles were cooled down from ambient temperature to -30 °C and heated again to room temperature with a constant heating rate of 2 °C/min. The freezing point of the test item was determined to be -25 °C at atmospheric pressure (1013 hPa).
Reference
Appearance of the Samples
Before the test the appearance of the test item was light yellow, viscous liquid. After the experiments the test item was unchanged in the crucible.
Results
Using a linear heating / cooling rate of 2 °C/min the freezing point of the test item was determined to be -25 °C (248 K).
Table 1. Summary of DSC results with the test item
Experiment 1 |
Experiment 2 |
Experiment 3 |
Mean |
Remark |
-25.44 |
-25.11 |
-25.02 |
-25 °C |
Glass transition temperature |
Description of key information
The freezing point of the test item was determined to be -25 °C.
Key value for chemical safety assessment
- Melting / freezing point at 101 325 Pa:
- -25 °C
Additional information
A study was conducted according to OECD TG 102, Regulation (EC) No 440/2008 method A.1 and EPA OPPTS 830.7200 to determine the freezing point of the test item using differential scanning calorimetry. The test item was weighed into an aluminium crucible under an inert atmosphere (nitrogen). Three tests were performed. As reference crucible, an empty aluminium crucible was used. The substance is a liquid at ambient conditions. Therefore, the crucibles were cooled down from ambient temperature to -30 °C and heated again to room temperature with a constant heating rate of 2 °C/min. The freezing point of the test item was determined to be -25 °C at atmospheric pressure (1013 hPa).
Information on Registered Substances comes from registration dossiers which have been assigned a registration number. The assignment of a registration number does however not guarantee that the information in the dossier is correct or that the dossier is compliant with Regulation (EC) No 1907/2006 (the REACH Regulation). This information has not been reviewed or verified by the Agency or any other authority. The content is subject to change without prior notice.
Reproduction or further distribution of this information may be subject to copyright protection. Use of the information without obtaining the permission from the owner(s) of the respective information might violate the rights of the owner.
