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Please be aware that this old REACH registration data factsheet is no longer maintained; it remains frozen as of 19th May 2023.

The new ECHA CHEM database has been released by ECHA, and it now contains all REACH registration data. There are more details on the transition of ECHA's published data to ECHA CHEM here.

Diss Factsheets

Administrative data

Endpoint:
appearance / physical state / colour
Type of information:
experimental study
Adequacy of study:
key study
Study period:
October 2009
Reliability:
1 (reliable without restriction)
Rationale for reliability incl. deficiencies:
other: Visual Observation

Data source

Reference
Reference Type:
study report
Title:
Unnamed
Year:
2009
Report date:
2009

Materials and methods

Test guideline
Qualifier:
no guideline followed
Principles of method if other than guideline:
Visual observation at room temperature
GLP compliance:
no

Test material

Constituent 1
Reference substance name:
NMSBA
IUPAC Name:
NMSBA
Constituent 2
Chemical structure
Reference substance name:
4-methanesulfonyl-2-nitrobenzoic acid
EC Number:
601-017-1
Cas Number:
110964-79-9
Molecular formula:
C8 H7 N1 O6 S1
IUPAC Name:
4-methanesulfonyl-2-nitrobenzoic acid
Details on test material:
Study performed on Commercial Batch n°30014009 which relates to NMSBA crude containing 15% water but in line with substance identity as described in Section 1.2

Analytical characterisation of the batch

SPECIFICATIONS METHODS RESULTS
Appearance Wet powder, LAM23/014/037 Accepted
white to greenish
Assay by titration >= 75.0 % LAM13/002/011.25 83,7 %
2-NMST by HPLC <= 3.0 % LAM13/002/011.46 0,9 %
Loss on drying by IR <= 20.0 % LAM13/002/011.26 15,0 %

The batch is in compliance with commercial specification

Results and discussion

Physical state at 20°C and 1013 hPa:
solid
Form / colour / odour
Form:
crystalline
Colour:
green almond
Odour:
odourless
Substance type:
organic

Applicant's summary and conclusion

Executive summary:

Visual observation at room temperature of crude NMSBA (containing 15% water) shows an odourless green almond crystalline solid.