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Please be aware that this old REACH registration data factsheet is no longer maintained; it remains frozen as of 19th May 2023.

The new ECHA CHEM database has been released by ECHA, and it now contains all REACH registration data. There are more details on the transition of ECHA's published data to ECHA CHEM here.

Diss Factsheets

Physical & Chemical properties

Particle size distribution (Granulometry)

Administrative data

Endpoint:
particle size distribution (granulometry)
Type of information:
experimental study
Adequacy of study:
key study
Study period:
2007-08-31
Reliability:
1 (reliable without restriction)
Rationale for reliability incl. deficiencies:
other: According to SOP Pulverrinne_3bar_vib30_gs; air.
Cross-reference
Reason / purpose for cross-reference:
reference to same study

Data source

Reference
Reference Type:
study report
Title:
Unnamed
Year:
2007
Report date:
2007

Materials and methods

Test guideline
Qualifier:
according to guideline
Guideline:
other: SOP_Pulverrinne_vib30_3bar_gs; air
Deviations:
no
Principles of method if other than guideline:
SOP name: Pulverrinne_3bar_vib30_gs
Equipment: Malvern Mastersizer 2000, unit: Scirocco 2000
Dispersing fluid: Air
GLP compliance:
no
Remarks:
According to ECHA Guidance (phys.chem. Studies), GLP compliance is not necessary.
Type of distribution:
volumetric distribution

Test material

Constituent 1
Chemical structure
Reference substance name:
2'-methylacetoacetanilide
EC Number:
202-267-0
EC Name:
2'-methylacetoacetanilide
Cas Number:
93-68-5
Molecular formula:
C11H13NO2
IUPAC Name:
N-(2-methylphenyl)-3-oxobutanamide
Test material form:
solid: particulate/powder
Remarks:
migrated information: powder
Details on test material:
Date of expiry: 11.12.2007 (statement of producer)
Storage: RT
Identity: Confirmed by H-NMR, IR-and mass spectrometry (LC/MS)
Appearance: White powder
Odour: Non-specific

Results and discussion

Particle sizeopen allclose all
Percentile:
D50
Mean:
48.2 µm
Remarks on result:
other: Migrated from fields under 'Mass median diameter' as D50 percentile. No source field for Standard deviation.
Percentile:
D10
Mean:
5.1 µm
St. dev.:
0.2
Percentile:
D50
Mean:
48.2 µm
St. dev.:
6.3
Percentile:
D90
Mean:
245.1 µm
St. dev.:
57.1

Applicant's summary and conclusion

Conclusions:
The median value D50 is = 48.2 µm.
Executive summary:

The study for particle size distribution was performed according to SOP Pulverrinne_3bar_vib30_gs. Method volumetric distribution.

The median value D50 for the particle size distribution of the test item is 48.2 µm, determined with Malvern Mastersizer 2000; unit Scirocco 2000, distribution in air.