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Diss Factsheets

Physical & Chemical properties

Melting point / freezing point

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Administrative data

Link to relevant study record(s)

Reference
Endpoint:
melting point/freezing point
Type of information:
experimental study
Adequacy of study:
key study
Study period:
From 03/05/2016 to 31/08/2016
Reliability:
1 (reliable without restriction)
Rationale for reliability incl. deficiencies:
guideline study
Reason / purpose for cross-reference:
reference to same study
Reason / purpose for cross-reference:
reference to same study
Qualifier:
according to guideline
Guideline:
OECD Guideline 102 (Melting point / Melting Range)
Deviations:
no
Qualifier:
according to guideline
Guideline:
EU Method A.1 (Melting / Freezing Temperature)
GLP compliance:
yes (incl. QA statement)
Remarks:
2015-07-28
Type of method:
differential scanning calorimetry
Key result
Decomposition:
yes
Remarks:
first range of decomposition temperature observed
Decomp. temp.:
> 150 - < 200 °C
Key result
Decomposition:
yes
Remarks:
Second range of decomposition temperature observed
Decomp. temp.:
> 225 - 275 °C
Conclusions:
No melting point of the test item was recorded from -110 °C to 600 °C. it was shown that a decomposition of the test item occurred from about 150 °C to 200 °C and from 225 °C to 275 °C.
Executive summary:
Melting point of Phosphonium, tetrakis(hydroxymethyl) -, sulphate (2:1), reaction products with 1-tetradecanamine and urea has been determined according to EC A.1 method and OECD test guideline 102 in compliance with GLP. Using Differential Scanning Calorimetry (DSC), No melting point was determined from -110°C to 600°C. Decomposition of the test item occurred from about 150 °C to 200 °C and from 225 °C to 275 °C.

Description of key information

No melting point was determined as the substance decomposed before melting

Key value for chemical safety assessment

Additional information

An experimental study, assessed as Klimisch 1, was selected as a key study. It was performed in compliance with GLP according to EC A.1. test method and OECD 102 guideline.