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Please be aware that this old REACH registration data factsheet is no longer maintained; it remains frozen as of 19th May 2023.

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Diss Factsheets

Physical & Chemical properties

Boiling point

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Administrative data

Link to relevant study record(s)

Reference
Endpoint:
boiling point
Type of information:
experimental study
Adequacy of study:
key study
Study period:
5th November 2015 to 11th May 2017
Reliability:
1 (reliable without restriction)
Rationale for reliability incl. deficiencies:
guideline study
Qualifier:
according to guideline
Guideline:
OECD Guideline 103 (Boiling Point)
Qualifier:
according to guideline
Guideline:
EU Method A.2 (Boiling Temperature)
GLP compliance:
yes (incl. QA statement)
Type of method:
method according to Siwoloboff
Specific details on test material used for the study:
Identity: RM1004998
Appearance: Yellow cloudy liquid
Storage conditions: Room temperature (15 to 25°C)
Batch number: 1023R26015
Purity: 99.7% on dry basis
Expiry date: 16th September, 2017
Key result
Boiling pt.:
> 213 °C
Atm. press.:
ca. 1 020 mBar
Decomposition:
yes
Decomp. temp.:
ca. 213 °C
Remarks on result:
not determinable

Decomposition occured at 213 °C; the item was observed to darken. No boiling took place upon continouation of heating to 350 °C.

Conclusions:
The substance was found to decompose at 213 °C, with the test material darkening. No boiling was observed upon further heating up to 360 °C.
Executive summary:

The boiling point of the substance was tested in accordance with OECD Guideline 103 and EU Method A.2 via a GLP certified laboratory, using the Siwoloboff method (barrometric pressure of 1020 mbar). The boiling point was undeterminable, when heating from room temperature up to 360 °C due to observed decomposition at 213 °C (darkening of the product). The substance did not proceed to boil after decomposition and continued heating.

Description of key information

The boiling point of the substance was tested in accordance with OECD Guideline 103 and EU Method A.2 via a GLP certified laboratory, using the Siwoloboff method (barrometric pressure of 1020 mbar). The boiling point was undeterminable, when heating from room temperature up to 360 °C due to observed decomposition at 213 °C (darkening of the product). The substance did not proceed to boil after decomposition and continued heating.

Key value for chemical safety assessment

Boiling point at 101 325 Pa:
213 °C

Additional information