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Please be aware that this old REACH registration data factsheet is no longer maintained; it remains frozen as of 19th May 2023.

The new ECHA CHEM database has been released by ECHA, and it now contains all REACH registration data. There are more details on the transition of ECHA's published data to ECHA CHEM here.

Diss Factsheets

Administrative data

Endpoint:
melting point/freezing point
Type of information:
experimental study
Adequacy of study:
key study
Study period:
23.06.2014
Reliability:
1 (reliable without restriction)
Rationale for reliability incl. deficiencies:
guideline study

Data source

Reference
Reference Type:
study report
Title:
Unnamed
Year:
2014
Report date:
2014

Materials and methods

Test guidelineopen allclose all
Qualifier:
according to guideline
Guideline:
EU Method A.1 (Melting / Freezing Temperature)
Deviations:
no
Qualifier:
according to guideline
Guideline:
OECD Guideline 102 (Melting point / Melting Range)
Deviations:
no
GLP compliance:
no
Type of method:
differential scanning calorimetry

Test material

Constituent 1
Chemical structure
Reference substance name:
N-{[1,1'-biphenyl]-2-yl}-N-(9,9-dimethyl-9H-fluoren-2-yl)-9,9'-spirobi[fluoren]-2-amine
EC Number:
700-681-0
Cas Number:
1364603-07-5
Molecular formula:
C52H37N
IUPAC Name:
N-{[1,1'-biphenyl]-2-yl}-N-(9,9-dimethyl-9H-fluoren-2-yl)-9,9'-spirobi[fluoren]-2-amine
Test material form:
solid

Results and discussion

Melting / freezing point
Key result
Melting / freezing pt.:
255.8 °C
Atm. press.:
1 013 hPa
Decomposition:
no
Sublimation:
no

Any other information on results incl. tables

It was concluded from the results of the DSC and capillary method that the test item showed a weak endothermal effect in the temperature range of 130 °C - 155 °C and a weak exothermic effect in the temperature range of 160 °C - 240 °C but remained solid and unchanged in its visual appearance up to its melting point of 255.8 °C ± 0.5 °C.

Applicant's summary and conclusion

Conclusions:
The melting point of the test item was determined to be 255.8 °C +/- 0.5 °C.
Executive summary:

The test item showed a weak endothermal effect in the temperature range of 130 °C - 150 °C and a weak exothermic effect in the temperature range of 160 °C - 240 °C but remained solid and unchanged in its visual appearance up to its melting point of 255.8 °C ± 0.5 °C.