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Physical & Chemical properties

Boiling point

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Administrative data

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Reference
Endpoint:
boiling point
Type of information:
experimental study
Adequacy of study:
key study
Study period:
17.07.2018 - 19.07.2018
Reliability:
1 (reliable without restriction)
Rationale for reliability incl. deficiencies:
guideline study
Qualifier:
according to guideline
Guideline:
OECD Guideline 103 (Boiling Point)
Version / remarks:
27th July 1995
Deviations:
no
GLP compliance:
no
Other quality assurance:
ISO/IEC 17025 (General requirements for the competence of testing and calibration laboratories)
Type of method:
differential scanning calorimetry
Specific details on test material used for the study:
lot/batch No.of test material: 1712001

Key result
Atm. press.:
1 008 mBar
Decomposition:
yes
Decomp. temp.:
ca. 353 °C
Remarks on result:
not determinable

To determine the boiling behaviour (three in dependent single measurements), the test item was measured by DSC between 5°C and 500°C with a heating rate of 10 K/min. For the measurement a partially capsulated crucible, typical for boiling point measurements,was used.

 

The test item No.: 5424/18 shows a boiling and/or thermal decomposition earliest at approx. 353°C (at 1008 mbar) according to the definition in the OECD guideline 103.

 

353°C (from first measurement)

353°C (from second measurement)

354°C (from third measurement)

From 353°C the test item shows a boiling and/or thermal decomposition with evaporation of the decomposition components.

The DSC measurements were confirmed by means of TGA measurements under the same measuring conditions.

 

The start of the area of boiling temperatures is defined by using the on-set temperature.

 

Description of key information

The test item MCC-5424/18 shows a boiling and/or thermal decomposition earliest at approx. 353 °C (at 1008 mbar) according to the definition in the OECD guideline 103.

Key value for chemical safety assessment

Additional information