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Please be aware that this old REACH registration data factsheet is no longer maintained; it remains frozen as of 19th May 2023.

The new ECHA CHEM database has been released by ECHA, and it now contains all REACH registration data. There are more details on the transition of ECHA's published data to ECHA CHEM here.

Diss Factsheets

Physical & Chemical properties

Particle size distribution (Granulometry)

Administrative data

Endpoint:
particle size distribution (granulometry)
Type of information:
experimental study
Adequacy of study:
key study
Study period:
2017
Reliability:
1 (reliable without restriction)
Rationale for reliability incl. deficiencies:
guideline study

Data source

Reference
Reference Type:
study report
Title:
Unnamed
Year:
2017

Materials and methods

Test guideline
Qualifier:
according to guideline
Guideline:
ISO 13320 (Particle size analysis - Laser diffraction methods)
GLP compliance:
not specified
Type of method:
Laser scattering/diffraction

Test material

Constituent 1
Chemical structure
Reference substance name:
1,1,1-trichloro-2-methyl-2-propanol hemihydrate
Cas Number:
6001-64-5
Molecular formula:
C4H7Cl3O H2O
IUPAC Name:
1,1,1-trichloro-2-methyl-2-propanol hemihydrate
Test material form:
solid: crystalline
Details on test material:
transparent and crystalline solid at ambient temperature

Results and discussion

Particle sizeopen allclose all
Key result
Percentile:
D10
Mean:
132.3 µm
St. dev.:
5.47
Key result
Percentile:
D50
Mean:
339.7 µm
St. dev.:
0.22
Key result
Percentile:
D90
Mean:
824.9 µm
St. dev.:
6.15

Applicant's summary and conclusion

Conclusions:
The test item Chlorobutanol Hemihydrate has the following particle size distribution according to the definition of ISO 13320:2009 and HSA-method (S) 13X11001.02. The volume percentages of D(10)-, D(50)- and D(90)- values are listed (see appendix 1 and table 1). A D90 value of 100 μm means that 90 vol % of the particles are smaller than 100 μm.
Executive summary:

The particle size distribution of the test item was determined with static laser light scattering according to ISO 13320:2009 and HSA-method (S) 13X11001.02.