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Please be aware that this old REACH registration data factsheet is no longer maintained; it remains frozen as of 19th May 2023.

The new ECHA CHEM database has been released by ECHA, and it now contains all REACH registration data. There are more details on the transition of ECHA's published data to ECHA CHEM here.

Diss Factsheets

Administrative data

Endpoint:
relative self-ignition temperature (solids)
Type of information:
experimental study
Adequacy of study:
key study
Study period:
27 September - 06 November 2001
Reliability:
1 (reliable without restriction)
Rationale for reliability incl. deficiencies:
guideline study

Data source

Reference
Reference Type:
study report
Title:
Unnamed
Year:
2002
Report date:
2002

Materials and methods

Test guideline
Qualifier:
according to guideline
Guideline:
EU Method A.16 (Relative Self-Ignition Temperature for Solids)
Deviations:
no
GLP compliance:
yes (incl. QA statement)

Test material

Constituent 1
Chemical structure
Reference substance name:
-
EC Number:
439-750-2
EC Name:
-
Cas Number:
183487-56-1
Molecular formula:
Hill formula: C17H19BrClNO3 CAS formula: C17H19BrClNO3
IUPAC Name:
(4aR*,8aR*)-1-bromo-4a,5,9,10,11,12- hexahydro-3-methoxy-11-methyl-6H-ben zofuro[3a,3,2-ef][2]benzazepin-6-one hydrochloride
Test material form:
solid: particulate/powder
Specific details on test material used for the study:
- Batch n°: RT002113G3A231
- Analytical purity: 92.9%
- Expiration date: 01 December 2001
- Storage condition: at room temperature

Results and discussion

Relative self-ignition temperature (solids)
Key result
Relative self-ignition temperature:
337 °C
Remarks on result:
other: Ambient pressure is anticipated
Remarks:
at atm. press. of 101.3 kPa

Any other information on results incl. tables

Applying a linear increase in temperature of about 0.5°C/min, T002113 showed an exothermic reaction starting at about 200°C. A Maximum temperature of about 529°C was measured in the sample cube during the exothermic reaction. At the end of the measurement, a rusty ash remained. T002113 shows a relative self-ignition temperature at about 337°C.

Applicant's summary and conclusion

Conclusions:
T002113 is auto-flammable under the conditions of the test.