Registration Dossier
Registration Dossier
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EC number: 248-383-5 | CAS number: 27277-00-5
Boiling point
Administrative data
Link to relevant study record(s)
- Endpoint:
- boiling point
- Type of information:
- experimental study
- Adequacy of study:
- key study
- Reliability:
- 1 (reliable without restriction)
- Rationale for reliability incl. deficiencies:
- other: The study was carried out in a laboratory accredited under GLP, however the study itself was not subject to GLP audit. The study was designed to be compatible with OECD TG 103 (1995) and Method A2 in Regulation (EC) No 440/2008 without deviations.
- Qualifier:
- according to guideline
- Guideline:
- OECD Guideline 103 (Boiling point/boiling range)
- Qualifier:
- according to guideline
- Guideline:
- EU Method A.2 (Boiling Temperature)
- GLP compliance:
- no
- Type of method:
- differential scanning calorimetry
- Boiling pt.:
- 364 °C
- Atm. press.:
- 100.4 kPa
- Conclusions:
- In a valid, reliable and conclusive study the boiling temperature of the test item was determined to be 364 °C (637 K) at 100.4 kPa.
- Executive summary:
To determine the boiling temperature of the test item a study was performed according to OECD TG 103 (1995) and Method A2 in Regulation (EC) No 440/2008. The boiling temperature of the test item was determined to be 364 °C (637 K) at 100.4 kPa. A minor discoloration/residue remained for all determinations performed under both an air atmosphere and a nitrogen atmosphere. This indicated possible thermal, as opposed to oxidative, decomposition during boiling.
- Endpoint:
- boiling point
- Type of information:
- experimental study
- Adequacy of study:
- supporting study
- Reliability:
- 1 (reliable without restriction)
- Rationale for reliability incl. deficiencies:
- other: The study was carried out in a laboratory accredited under GLP, however the study itself was not subject to GLP audit. The study was designed to be compatible with OECD TG 103 (1995) and Method A2 in Regulation (EC) No 440/2008 without deviations.
- Qualifier:
- according to guideline
- Guideline:
- OECD Guideline 103 (Boiling point/boiling range)
- Qualifier:
- according to guideline
- Guideline:
- EU Method A.2 (Boiling Temperature)
- GLP compliance:
- no
- Type of method:
- differential scanning calorimetry
- Boiling pt.:
- 364 °C
- Atm. press.:
- 98.7 kPa
- Conclusions:
- In a valid, reliable and conclusive study the boiling temperature of the test item was determined to be 364 °C (637 K) at 98.7 kPa.
- Executive summary:
To determine the boiling temperature of the test item a study was performed according to OECD TG 103 (1995) and Method A2 in Regulation (EC) No 440/2008. The boiling temperature of the test item was determined to be 364 °C (637 K) at 98.7 kPa. A minor discoloration/residue remained for all determinations performed under both an air atmosphere and a nitrogen atmosphere. This indicated possible thermal, as opposed to oxidative, decomposition during boiling.
Referenceopen allclose all
Thermographic data (extrapolated endotherm onset temperatures), determinations 1 -6:
Sample number
|
Interpretation |
Temperature |
|
°C |
K |
||
1 |
Boiling temperature |
363.90 |
637 |
2 |
364.07 |
637 |
|
3 |
Maximum rate of evaporation of the test item from an open test system |
328.73 |
602 |
4 |
325.77 |
599 |
|
5 |
329.16 |
602 |
|
6 |
311.89 |
585 |
|
Thermographic data (extrapolated endotherm onset temperatures), determinations 1 -6:
Sample number
|
Interpretation |
Temperature |
|
°C |
K |
||
1 |
Boiling temperature |
364.10 |
637 |
2 |
364.14 |
637 |
|
3 |
Maximum rate of evaporation of the test item from an open test system |
331.17 |
604 |
4 |
333.09 |
606 |
|
5 |
318.76 |
592 |
|
6 |
313.56 |
587 |
|
Description of key information
364 °C, OECD 103, GLP, DSC, O'Connor 2015
Key value for chemical safety assessment
- Boiling point at 101 325 Pa:
- 364 °C
Additional information
In a valid, reliable and conclusive study the boiling temperature of the test item was determined to be 364 °C at 100.4 kPa. In a supporting study, the boiling temperature of the test item was determined to be 364 °C at 98.7 kPa.
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