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Please be aware that this old REACH registration data factsheet is no longer maintained; it remains frozen as of 19th May 2023.

The new ECHA CHEM database has been released by ECHA, and it now contains all REACH registration data. There are more details on the transition of ECHA's published data to ECHA CHEM here.

Diss Factsheets

Administrative data

Endpoint:
water solubility
Type of information:
experimental study
Adequacy of study:
other information
Reliability:
2 (reliable with restrictions)
Rationale for reliability incl. deficiencies:
other: Basic data given

Data source

Referenceopen allclose all

Reference Type:
study report
Title:
Unnamed
Year:
1991
Report date:
1991
Reference Type:
study report
Title:
Unnamed
Year:
1991
Report date:
1991

Materials and methods

Principles of method if other than guideline:
flask method
GLP compliance:
yes

Test material

Constituent 1
Chemical structure
Reference substance name:
1,3-dichlorobut-2-ene
EC Number:
213-138-3
EC Name:
1,3-dichlorobut-2-ene
Cas Number:
926-57-8
Molecular formula:
C4H6Cl2
IUPAC Name:
1,3-dichlorobut-2-ene
Details on test material:
- Name of test material (as cited in study report): 2-Butene, E/Z-1,3-Dichlorbuten-2
- Analytical purity: 99.1 %

Results and discussion

Any other information on results incl. tables

A determination of water solubility was not possible for the following reasons:

1. When preliminary tests were performed, disappearance of the 2 phases was observed on prolonged standing.

2. A reduction of the stirring time to 4 hours and immediate analysis of the content showed that 1,3-dichlorobut-2 -ene content decreased by 26% between the first and eighth injections.

3. In a subsequent main experiment using 10 times the originally weighed-in amount of test material, the mixture was homogeneous after half of the prescribed stirring time, which indicated hydrolysis and solubilization.

Applicant's summary and conclusion