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Physical & Chemical properties

Melting point / freezing point

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Reference
Endpoint:
melting point/freezing point
Type of information:
experimental study
Adequacy of study:
key study
Study period:
21/03/2016 - 21/03/2016
Reliability:
1 (reliable without restriction)
Rationale for reliability incl. deficiencies:
test procedure in accordance with national standard methods
Justification for type of information:
Experimental test result performed using Standard method of analysis
Qualifier:
according to guideline
Guideline:
other: as mention below
Principles of method if other than guideline:
The freezing point of a pure sample is the temperature at which transition from liquid to solid state takes place at atmospheric pressure. The Freezing point determination of test item was done using crushed ice-salt cooling bath.
GLP compliance:
no
Type of method:
other: crushed ice-salt cooling bath
Specific details on test material used for the study:
- Name of test material: undec-10-enal
- Molecular weight: 168.278 g/mol
- Molecular formula: C11-H20-O
- Substance type: Organic
- Physical state: Liquid
- Analytical purity:98.82% (GLC)
- Lot/batch No.:KC/C11/1412051
- Stability under test conditions: Stable in recommended storage conditions
- Storage condition of test material: Store in cool place. Keep container tightly closed in a dry and well-ventilated place.

Key result
Melting / freezing pt.:
< -16.6 °C
Atm. press.:
971.4 hPa
Decomposition:
no
Sublimation:
no
Remarks on result:
other: No other detail available

TEST DESCRIPTION AND RESULTS

Method Details

Observations 

Remarks if, any

Method

Freezing Temperature Method

 

 

Principle of Freezing point test

The freezing point of a pure sample is the temperature at which transition from liquid to solid state takes place at atmospheric pressure. 

 

-

Quantity of test item used

g

1.0

-

Type of cooling bath used

·        Cold Water

·        Crushed Ice

·        Crushed Ice-Salt

·        Dry Ice

·        Other (specify)

Crushed ice-salt

-

Type and model no. of temperature sensor used

·        Glass thermometer

·        Thermocouple

·        Thermistor

·        Other (specify)

Thermistor probe

-

Atmospheric pressure

hPa

971.4

-

Freezing point

°C

< -16.6 °C

-

 

Conclusions:
The Freezing point of test chemical was determined with crushed ice-salt cooling bath and the freezing point was inferred to be< -16.6 °Cat 971.4 hPa.
Executive summary:

The Freezing point of test chemical was determined with crushed ice-salt cooling bath and the freezing point was inferred to be< -16.6 °Cat 971.4 hPa.

Description of key information

The Freezing point of test chemical was determined with crushed ice-salt cooling bath and the freezing point was inferred to be< -16.6 °Cat 971.4 hPa.

Key value for chemical safety assessment

Melting / freezing point at 101 325 Pa:
-16.6 °C

Additional information

The Freezing point of test chemical was determined with crushed ice-salt cooling bath and the freezing point was inferred to be< -16.6 °Cat 971.4 hPa.