Registration Dossier

Data platform availability banner - registered substances factsheets

Please be aware that this old REACH registration data factsheet is no longer maintained; it remains frozen as of 19th May 2023.

The new ECHA CHEM database has been released by ECHA, and it now contains all REACH registration data. There are more details on the transition of ECHA's published data to ECHA CHEM here.

Diss Factsheets

Physical & Chemical properties

Boiling point

Currently viewing:

Administrative data

Link to relevant study record(s)

Reference
Endpoint:
boiling point
Type of information:
experimental study
Adequacy of study:
key study
Study period:
29 November 2017 to 20 March 2018
Reliability:
1 (reliable without restriction)
Rationale for reliability incl. deficiencies:
guideline study
Qualifier:
according to guideline
Guideline:
EU Method A.2 (Boiling Temperature)
Version / remarks:
EC No 440/2008
Deviations:
no
Qualifier:
according to guideline
Guideline:
OECD Guideline 103 (Boiling Point)
Version / remarks:
27 July 1995
Deviations:
no
GLP compliance:
yes (incl. QA statement)
Type of method:
differential scanning calorimetry
Specific details on test material used for the study:
- Batch No.of test material: PFW160141
- Purity: 99.5%
- Expiration date of the lot/batch: 30 December 2018
- Stability under test conditions: Room temperature in the dark
Key result
Boiling pt.:
217 °C
Atm. press.:
>= 98.5 - <= 101 kPa
Decomposition:
no
Remarks on result:
other: mean of 5 runs

Thermographic Data

Thermal Event

Interpretation

Temperature (°C)

Determination 1

Determination 2

Determination 3

Endotherm

Boiling Point Onset

200.52

217.50

217.31

Thermal Event

Interpretation

Temperature (°C)

Determination 4

Determination 5

Determination 6

Endotherm

Boiling Point Onset

216.99

216.23

216.22

Atmospheric pressure:  Determinations 1 & 2:           101.0 kPa
                                    Determinations 3 to 6:           98.5 kPa

Mean boiling temperature: 217 ±1.0°C (490±1.0K)

The result for Sample 1 was a wide, multi-endotherm and was out of agreement with the rest of the thermograms which were in agreement. Therefore, Sample 1 has not been used in determination of the endpoint.

Conclusions:
The boiling point of the test item has been determined to be 217 ± 1.0 °C (490 ± 1.0 K) at 98.5 to 101.0 kPa.

Description of key information

A GLP-compliant study was performed according to OECD guideline 103 and EU Method A.2. The boiling point of the test substance was determined to be 217 ± 1.0 °C or 490 ± 1.0 K at 98.5 to 101.0 kPa (K1, Covance, 2019).

Key value for chemical safety assessment

Additional information

The boiling point of the test substance was found to be 217 ± 1.0 °C at 98.5 - 101.0 kPa