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Please be aware that this old REACH registration data factsheet is no longer maintained; it remains frozen as of 19th May 2023.

The new ECHA CHEM database has been released by ECHA, and it now contains all REACH registration data. There are more details on the transition of ECHA's published data to ECHA CHEM here.

Diss Factsheets

Administrative data

Endpoint:
melting point/freezing point
Type of information:
experimental study
Adequacy of study:
key study
Study period:
2015
Reliability:
2 (reliable with restrictions)
Rationale for reliability incl. deficiencies:
other: according to valid method (DSC)

Data source

Reference
Reference Type:
study report
Title:
Unnamed
Year:
2015
Report date:
2015

Materials and methods

Principles of method if other than guideline:
Capillary method for melting point
Differential Scanning Calorimetry for decomposition
GLP compliance:
not specified
Type of method:
thermal analysis

Test material

Constituent 1
Chemical structure
Reference substance name:
2,5-dichloroanilinium chloride
EC Number:
251-620-5
EC Name:
2,5-dichloroanilinium chloride
Cas Number:
33663-41-1
Molecular formula:
C6H5Cl2N.ClH
IUPAC Name:
2,5-dichloroanilinium chloride

Results and discussion

Melting / freezing point
Melting / freezing pt.:
187 °C
Atm. press.:
ca. 1 atm
Decomposition:
yes
Decomp. temp.:
>= 270 °C
Remarks on result:
other: The product starts to decompose in the sealed vial at 270°C with a mean energy of 108 J/g.Due to the irregular base line, there is considerable uncertainty in the decomposition energy.The endothermic peak between 188°C and 262°C is the main melting point

Applicant's summary and conclusion

Conclusions:
The tested melting point is 187°C.
Executive summary:

The melting point was determined using a capillary method device.

The decomposition was determeined by Differential Scanning Calorimetry.