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Physical & Chemical properties

Particle size distribution (Granulometry)

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Reference
Endpoint:
particle size distribution (granulometry)
Type of information:
experimental study
Adequacy of study:
key study
Study period:
26/09/2018-02/10/2018
Reliability:
2 (reliable with restrictions)
Rationale for reliability incl. deficiencies:
other: Non-GLP study
Qualifier:
according to guideline
Guideline:
other: CIPAC MT 187 2003
GLP compliance:
no
Type of method:
Laser scattering/diffraction
Mean:
8.062 µm
Remarks on result:
other: Surface weighed Mean D [3,2]
Mean:
17.693 µm
Remarks on result:
other: Volume weighed Mean D [4,3]
Conclusions:
The results are reported below:
Concentration: 0.0186 %Vol;
Span: 1.509,
Uniformity: 0.463;
Result units: Volume;
Specific surface area: 0.744 m2/g;
Surface weighed Mean D [3,2]: 8.062 μm;
Volume weighed Mean D [4,3]: 17.693 μm.
Executive summary:

The method describes the procedure for determining the granulometric distribution by laser diffractometry in different matrices. The laser diffraction technique is based on the principle that particles, passing through a laser beam, diffuse light at an angle that is related to their size. As the particle size decreases, the observed scattering angle increases logarithmically. The scattering intensity also depends on the particle size and decreases, with a good approximation, in relation to the surface of the particle cross-section. By simplifying, large particles spread light with narrow angles and high intensity, while small particles with wider angles and low intensities. The instrument is able to relate the scattering angle and intensity to the granulometric distribution of the material under examination.

The results are reported below:

Concentration: 0.0186 %Vol;

Span: 1.509,

Uniformity: 0.463;

Result units: Volume;

Specific surface area: 0.744 m2/g;

Surface weighed Mean D [3,2]: 8.062 μm;

Volume weighed Mean D [4,3]: 17.693 μm.

Description of key information

The results are reported below:

Concentration: 0.0186 %Vol;

Span: 1.509,

Uniformity: 0.463;

Result units: Volume;

Specific surface area: 0.744 m2/g;

Surface weighed Mean D [3,2]: 8.062 μm;

Volume weighed Mean D [4,3]: 17.693 μm.

Additional information

The method used is CIPAC MT 187 – Particle size analysis by laser diffraction