Registration Dossier

Diss Factsheets

Administrative data

Endpoint:
density
Remarks:
Density types indicated (migrated information): pour density; tap density
Type of information:
experimental study
Adequacy of study:
key study
Reliability:
2 (reliable with restrictions)
Rationale for reliability incl. deficiencies:
other: OECD guideline study, conducted to a high standard but not certified as being to GLP.

Data source

Reference
Reference Type:
study report
Title:
Unnamed
Year:
2015

Materials and methods

Test guideline
Qualifier:
according to guideline
Guideline:
OECD Guideline 109 (Density of Liquids and Solids)
Deviations:
no
GLP compliance:
no
Type of method:
other: Pour and tap densities for solids

Test material

Constituent 1
Chemical structure
Reference substance name:
1-hydroxy-2,2,6,6-tetramethylpiperidin-4-yl benzoate
EC Number:
807-702-3
Cas Number:
3225-26-1
Molecular formula:
C16H22NO3
IUPAC Name:
1-hydroxy-2,2,6,6-tetramethylpiperidin-4-yl benzoate
Test material form:
solid: crystalline
Details on test material:
- Material name: 4-hydroxyTEMPObenzoate
- Physical state: solid.
- Analysis date: 18th December 2014
- Analytical purity: 95.7 %.
- Impurities (identity and concentrations): triethylamine (0.56 %); 4-hydroxy TEMPO (0.8 %); deoxygenated benzoyl TEMPO (0.21 %); benzoic acid anhydride (1.48 %).
- Composition of test material, percentage of components: 95.7 % benzoyl TEMPO.
- Isomers composition: not applicable.
- Purity test date: 18 December 2014.
- Lot/batch No.: GP209
- Manufacturing date: 15/12/2014
- Expiration / re-test date of the lot/batch: 15/12/2015
- Stability under test conditions: stable.
- Storage condition of test material: Store in sealed container in cool dry place, away from heat and sunlight.

Results and discussion

Densityopen allclose all
Type:
pour density
Density:
0.4 g/L
Temp.:
20 °C
Type:
tap density
Density:
0.55 g/L
Temp.:
20 °C

Applicant's summary and conclusion

Executive summary:

The average pour density of benzoyl TEMPO is 0.400 g/mL

The average tap density of benzoyl TEMPO is 0.550 g/mL