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Diss Factsheets

Physical & Chemical properties

Melting point / freezing point

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Administrative data

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Endpoint:
melting point/freezing point
Type of information:
experimental study
Adequacy of study:
key study
Study period:
17 Dec 2018 to 25 Jan 2019
Reliability:
1 (reliable without restriction)
Rationale for reliability incl. deficiencies:
guideline study
Qualifier:
according to guideline
Guideline:
EU Method A.1 (Melting / Freezing Temperature)
Version / remarks:
March 04, 2016
Deviations:
no
Qualifier:
according to guideline
Guideline:
OECD Guideline 102 (Melting point / Melting Range)
Version / remarks:
July 27, 1995
Deviations:
no
Qualifier:
according to guideline
Guideline:
EPA OPPTS 830.7200 (Melting Point / Melting Range)
Version / remarks:
March 1998
Deviations:
no
GLP compliance:
yes (incl. QA statement)
Type of method:
differential scanning calorimetry
Specific details on test material used for the study:
Physical Description: White powder
Purity/Composition: 99.2%
Storage Conditions: At room temperature protected from light desiccated
Key result
Melting / freezing pt.:
94.9 °C
Atm. press.:
1 013.25 Pa
Conclusions:
The melting temperature of Esacure A 198 were determined by DSC.

The melting temperature of the test item was 94.9°C (368.0K).
Executive summary:

In this guideline (OECD 102) study, conducted with GLP certification, the melting point of the test substance (EC 466-080-8) was found to be <94.9 °C at 1013.25 hPa.

Endpoint:
melting point/freezing point
Type of information:
experimental study
Adequacy of study:
supporting study
Study period:
21 September 2006 to 17 October 2006
Reliability:
1 (reliable without restriction)
Rationale for reliability incl. deficiencies:
guideline study
Qualifier:
according to guideline
Guideline:
EU Method A.1 (Melting / Freezing Temperature)
Version / remarks:
EC's Classilication, Packaging & Labelling 01 Dangerous Substances in the European Union Part 2, Testing Methods, Jan97. Directive 92/69/EC (Annex V to Directive 67/548/EC)
GLP compliance:
yes (incl. QA statement)
Type of method:
capillary method
Specific details on test material used for the study:
Product Name: LFC 2098
Special Hazards: None specified
Appearance: Sample observed to be a white powder (determined by Chilworth Technology Ltd).
Melting / freezing pt.:
97.7 °C
Decomposition:
no
Sublimation:
no
Melting / freezing pt.:
97.6 °C
Decomposition:
no
Sublimation:
no

Result : 97.7 °C (mean of 2 runs)

The mean of at least two measurements, which are in the range of the estimated accuracy, is reported as the melting temperature.

If the difference between the temperature at the beginning and at the final stage of melting is within the limits of the accuracy of the method, the temperature at the final stage of melting is taken as the melting temperature, otherwise the two temperatures are reported.

If the substance decomposes or sublimes belore the melting temperature is reached, the temperature at which the effect is observed shall be reported.

Conclusions:
Result : 97.7°C (mean of 2 runs)
Executive summary:

In this guideline study (EU Method A.1) the melting point of the test substance (EC 466-080-8) was shown to be 97.7 °C.

Description of key information

Study conducted to recognised testing guidelines with GLP certification.

Key value for chemical safety assessment

Melting / freezing point at 101 325 Pa:
94.9 °C

Additional information