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Diss Factsheets

Administrative data

Endpoint:
water solubility
Type of information:
experimental study
Adequacy of study:
key study
Study period:
Experimental starting date: 21 February 2019 Experimental completion date: 09 March 2019
Reliability:
1 (reliable without restriction)

Data source

Reference
Reference Type:
study report
Title:
Unnamed
Year:
2019
Report date:
2019

Materials and methods

Test guidelineopen allclose all
Qualifier:
according to guideline
Guideline:
EU Method A.6 (Water Solubility)
Deviations:
no
Qualifier:
according to guideline
Guideline:
OECD Guideline 105 (Water Solubility)
Deviations:
no
GLP compliance:
yes
Type of method:
flask method

Test material

Constituent 1
Chemical structure
Reference substance name:
Benzenesulfonic acid, C10-24-branched and linear alkyl derivs., magnesium salts, overbased
EC Number:
948-935-1
Molecular formula:
Molecular formula cannot be determined for this UVCB substance
IUPAC Name:
Benzenesulfonic acid, C10-24-branched and linear alkyl derivs., magnesium salts, overbased
Specific details on test material used for the study:
Identification: T106D
Appearance/Physical state:amber brown viscous liquid
Chemical description:Magnesium long-chain alkaryl sulphonate
Batch:R18 14728
Purity:100% (UVCB)
Expiry date:08 October 2020
Storage conditions:room temperature, in the dark

Results and discussion

Water solubility
Key result
Water solubility:
< 0.001 other: gTOC/L
Temp.:
20 °C
pH:
>= 6.2 - <= 6.9

Any other information on results incl. tables

Results

Preliminary Test

The preliminary result of the water solubility at 20.0 ± 0.5 °C was less than 1 x 10-3gTOC/L. The solution had a pH of 6.7.

Definitive Test

The concentrations relating to the sample solutions are shown in the following table:

Solution

Concentration (mgTOC/L)

A

B

Mean

Matrix blank

0.2707

0.2443

0.2575

Sample 1

0.4925

0.5870

0.5398

Sample 2

0.5043

0.4862

0.4953

Sample 3

0.5844

0.5324

0.5584

The concentration (g/L) of test item in the sample solutions is shown in the following table:

Sample Number

Time Shaken at

~ 30 ºC (hours)

Concentration (gTOC/L)

Solution pH

1

24

2.82 x 10-4

6.9

2

48

2.38 x 10-4

6.6

3

72

3.01 x 10-4

6.2

Mean concentration:  2.74 x 10-4gTOC/L at 20.0 ± 0.5 ºC
Overall result:             <1 x 10-3gTOC/L

Applicant's summary and conclusion

Conclusions:
The water solubility of the test item has been determined to be less than 1 x 10E-3 gTOC/L of solution at 20.0 ± 0.5 °C.
Executive summary:

The determination was carried out by the flask method, using a procedure designed to be compatible with Method A.6 Water Solubility of Commission Regulation (EC) No 440/2008 of 30 May 2008 and Method 105 of the OECD Guidelines for Testing of Chemicals, 27 July 1995.

Conclusion

The water solubility of the test item has been determined to be less than 1 x 10-3 gTOC/L of solution at 20.0 ± 0.5 °C.