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Boiling point

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Reference
Endpoint:
boiling point
Type of information:
experimental study
Adequacy of study:
key study
Reliability:
1 (reliable without restriction)
Rationale for reliability incl. deficiencies:
guideline study
Qualifier:
according to guideline
Guideline:
OECD Guideline 103 (Boiling Point)
Version / remarks:
Due to the nature of the sample, boiling point was determined by thermogravimetric analysis (TGA), which is a
deviation from OECD Guidelines for The Testing of Chemicals, 103, July 27 1995.
GLP compliance:
yes (incl. QA statement)
Type of method:
other: thermogravimetric analysis (TGA)
Boiling pt.:
> 128 - < 145 °C
Atm. press.:
101.2 kPa
Decomposition:
no
Remarks on result:
other:
Remarks:
First boiling point
Boiling pt.:
296 °C
Atm. press.:
101.2 kPa
Decomposition:
no
Remarks on result:
other:
Remarks:
Second boiling point

TGA results indicate that the sample has several components boiling at different temperatures. The lowest major boiling component has a boiling point of 296°C (average) that is not completely resolved from a higher boiling component. It is possible the sample is decomposing while boiling at the higher temperature boiling point. There is also a minor lower boiling component comprising approximately 5% of the sample with a boiling point in the 128 to 145°C range that is not well-resolved.

Conclusions:
Boiling point of 4,4'-Isopropylidenediphenol, oligomeric reaction products with 1-chloro-2,3-epoxypropane, reaction products with 3-aminopropyldiethylamine and 2-piperazin-1-ylethylamine was determined using thermogravimetric analysis (TGA). Material has several components with different boiling point. 5% of the sample shower boiling point in the 128 to 145°C range that is not well-resolved. The lowest major boiling component has a boiling point of 296°C (average) that is not
completely resolved from a higher boiling component.
Executive summary:

Boiling point of 4,4'-Isopropylidenediphenol, oligomeric reaction products with 1-chloro-2,3-epoxypropane, reaction products with 3-aminopropyldiethylamine and 2-piperazin-1-ylethylamine was determined using thermogravimetric analysis (TGA). Material has several components with different boiling point. 5% of the sample shower boiling point in the 128 to 145°C range that is not well-resolved. The lowest major boiling component has a boiling point of 296°C (average) that is not

completely resolved from a higher boiling component.

Description of key information

Boiling point of 4,4'-Isopropylidenediphenol, oligomeric reaction products with 1-chloro-2,3-epoxypropane, reaction products with 3-aminopropyldiethylamine and 2-piperazin-1-ylethylamine was determined using thermogravimetric analysis (TGA). Material has several components with different boiling point. 5% of the sample shower boiling point in the 128 to 145°C range that is not well-resolved. The lowest major boiling component has a boiling point of 296°C (average) that is not

completely resolved from a higher boiling component.

Key value for chemical safety assessment

Boiling point at 101 325 Pa:
296 °C

Additional information