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Physical & Chemical properties

Particle size distribution (Granulometry)

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Reference
Endpoint:
particle size distribution (granulometry)
Type of information:
experimental study
Adequacy of study:
key study
Study period:
28 June 2019
Reliability:
1 (reliable without restriction)
Rationale for reliability incl. deficiencies:
guideline study
Qualifier:
according to guideline
Guideline:
OECD Guideline 110 (Particle Size Distribution / Fibre Length and Diameter Distributions) - Method B: Fibre Length and Diameter Distributions
Version / remarks:
1981
Qualifier:
according to guideline
Guideline:
EPA OPPTS 830.7520 (Particle Size, Fiber Length, and Diameter Distribution)
Version / remarks:
1996
Qualifier:
according to guideline
Guideline:
ISO 13320 (Particle size analysis - Laser diffraction methods)
Version / remarks:
2009
GLP compliance:
no
Type of method:
Laser scattering/diffraction
Type of particle tested:
other: fine fraction passing through a 1000 µm sieve
Type of distribution:
volumetric distribution
Mass median aerodynamic diameter:
16.59 µm
Percentile:
D50
Mean:
16.59 µm
Remarks on result:
other: fine fraction
Percentile:
D10
Mean:
1.37 µm
Remarks on result:
other: fine fraction
Percentile:
D90
Mean:
179.48 µm
Remarks on result:
other: fine fraction

One test series of 3 measurements was performed with the fine fraction of the test item.

A graph was created which shows the results. On the left y-axis the fraction distribution and on the right y-axis the cumulative distribution is shown.

A coarse fraction greater than 1000 µm of 79.3 % (wt.) and a fine fraction of less than 1000 µm of 20.7 % (wt.) was found. The fine fraction (<1000 µm) of the test item has a median particle size (D50) of 17 µm, which was determined by laser diffraction measurement according to ISO 13320 (2009) and OECD 110 (1981).

Conclusions:
The mass median diameter (D50) of the test item is 16.59 µm.
Executive summary:

The particle size of the test item was evaluated in an experimental study using the laser diffraction method according to the OECD guideline 110 (1981) and ISO 13320 (2009).

The following results were obtained:

D10 = 1.37 µm

D50 = 16.59 µm (mass median diameter)

D90 = 179.48 µm

Description of key information

D50 of the fine fraction (20.7 % w/w) is 16.59 µm .

Additional information

OECD guideline 110 (1981) and ISO 13320 (2009).