Registration Dossier
Registration Dossier
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EC number: 247-665-5 | CAS number: 26401-86-5
Melting point / freezing point
Administrative data
Link to relevant study record(s)
- Endpoint:
- melting point/freezing point
- Type of information:
- experimental study
- Adequacy of study:
- key study
- Study period:
- Not specified
- Reliability:
- 2 (reliable with restrictions)
- Rationale for reliability incl. deficiencies:
- guideline study with acceptable restrictions
- Qualifier:
- according to guideline
- Guideline:
- OECD Guideline 102 (Melting point / Melting Range)
- Version / remarks:
- 1995
- Deviations:
- yes
- Remarks:
- The samples were not permanently stirred but in regular time step manually
- GLP compliance:
- no
- Type of method:
- method to determine freezing temperature
- Key result
- Melting / freezing pt.:
- < -21 °C
- Conclusions:
- Under the conditions of this study, the freezing point of the test material was <-21°C.
- Executive summary:
The freezing point of the test material was investigated in accordance with the standardised guideline OECD 102, but without continuous stirring.
Ca. 50 g of the test material was placed in a deep freezer at -21°C The sample was stirred manually and observed for any signs of freezing in regular time steps. At the first signs of solidification / precipitation the temperature was determined by a thermometer.
Under the conditions of this study, the freezing point of the test material was <-21°C.
Reference
Description of key information
Under the conditions of the study, the freezing point of the test material was <-21°C.
Key value for chemical safety assessment
- Melting / freezing point at 101 325 Pa:
- -21 °C
Additional information
The freezing point of the test material was investigated in accordance with the standardised guideline OECD 102, but without continuous stirring. The study was awarded a reliability score of 2 in accordance with the criteria set forth by Klimisch et al. (1997).
Ca. 50 g of the test material was placed in a deep freezer at -21°C The sample was stirred manually and observed for any signs of freezing in regular time steps. At the first signs of solidification / precipitation the temperature was determined by a thermometer.
Under the conditions of this study, the freezing point of the test material was <-21°C.
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