Zinc bis(N-ethyl-N-phenyldithiocarbamate)

Boiling point

Link to relevant study record(s)

Reference

Endpoint:

boiling point

Type of information:

experimental study

Adequacy of study:

key study

Reliability:

1 (reliable without restriction)

Rationale for reliability incl. deficiencies:

guideline study

Qualifier:

according to guideline

Guideline:

EU Method A.2 (Boiling Temperature)

Deviations:

no

Qualifier:

according to guideline

Guideline:

other: ASTM E 472-86

Deviations:

no

Qualifier:

according to guideline

Guideline:

other: DIN 51007

Version / remarks:

2009

Deviations:

no

Qualifier:

according to guideline

Guideline:

other: DIN 53171

Deviations:

no

GLP compliance:

yes

Type of method:

differential scanning calorimetry

Specific details on test material used for the study:

Batch number: CN61204501
Content: 95.5%
Physical condition: white powder
Expiration date: 2017-12-04
Storage: Room temperature

Atm. press.:

>= 1 010 - <= 1 012 hPa

Decomposition:

no

Remarks on result:

other: no boiling up to 300°C

The atmospheric pressure at the time of measurement was 1010 and 1012 hPa. At about 142 °C, 208 °C and 306 °C were three small endothermic effects. The energy of these effects is too small for a boiling. There is no boiling up to a temperature of 300 °C.

Conclusions:

Boiling Temperature to Vulkacit P Extra N was determined according to EC No. 440/2008 A.2 showing no boiling up to 300°C.

Executive summary:

The boiling temperature to Vulkacit P Extra N was determined with the DCS-method described in ASTM E 472-86 and DIN 51007:1994. A sample was placed in a crucible made of aluminum and closed with a cap with a hole from about 0.5 mm. This hole was covered by a sphere from 1.5 mm diameter. The crucible with the substance and a reference crucible were subjected to the same controlled temperature program. The sample was heated at a linear rate of 10 K/min from 40 °C up to 400 °C. The measurement was recorded electronically. The measurement was done twice.

The atmospheric pressure at the time of measurement was 1010 and 1012 hPa. At about 142 °C, 208 °C and 306 °C were three small endothermic effects. The energy of these effects is too small for a boiling. There is no boiling up to a temperature of 300 °C.

Description of key information

The boiling temperature to Vulkacit P Extra N was determined with the DCS-method described in ASTM E 472-86 and DIN 51007:1994. A sample was placed in a crucible made of aluminum and closed with a cap with a hole from about 0.5 mm. This hole was covered by a sphere from 1.5 mm diameter. The crucible with the substance and a reference crucible were subjected to the same controlled temperature program. The sample was heated at a linear rate of 10 K/min from 40 °C up to 400 °C. The measurement was recorded electronically. The measurement was done twice.

The atmospheric pressure at the time of measurement was 1010 and 1012 hPa. At about 142 °C, 208 °C and 306 °C were three small endothermic effects. The energy of these effects is too small for a boiling. There is no boiling up to a temperature of 300 °C.