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EC number: 947-727-8 | CAS number: 568591-00-4
Boiling point
Administrative data
- Endpoint:
- boiling point
- Type of information:
- experimental study
- Adequacy of study:
- key study
- Study period:
- 11 Dec - 18 Dec 2017
- Reliability:
- 1 (reliable without restriction)
- Rationale for reliability incl. deficiencies:
- guideline study
- Remarks:
- GLP guideline study
Data source
Reference
- Reference Type:
- study report
- Title:
- Unnamed
- Year:
- 2 018
- Report date:
- 2018
Materials and methods
Test guidelineopen allclose all
- Qualifier:
- according to guideline
- Guideline:
- EU Method A.2 (Boiling Temperature)
- Version / remarks:
- 2008
- Deviations:
- no
- Qualifier:
- according to guideline
- Guideline:
- OECD Guideline 103 (Boiling Point)
- Version / remarks:
- 1995
- Deviations:
- no
- GLP compliance:
- yes (incl. QA statement)
- Remarks:
- Italian Ministry of Health, Rome, Italy
- Type of method:
- differential scanning calorimetry
Test material
- Reference substance name:
- Reaction mass of 2-ethyl-4-methyl-1H-imidazole-1-propiononitrile and 2-ethyl-5-methyl-1H-imidazole-1-propiononitrile
- EC Number:
- 947-727-8
- Cas Number:
- 568591-00-4
- Molecular formula:
- C9H13N3
- IUPAC Name:
- Reaction mass of 2-ethyl-4-methyl-1H-imidazole-1-propiononitrile and 2-ethyl-5-methyl-1H-imidazole-1-propiononitrile
Constituent 1
Results and discussion
Boiling point
- Boiling pt.:
- 265 °C
- Remarks on result:
- other: No details on pressure provided.
Any other information on results incl. tables
First test:
- sample amount: 6.35 mg
- crucible: Aluminum, lid with a 50 μm hole
- heating rate: 5 °C/min
- temperature range: 30-500 °C
- atmosphere: N2 flow, 20 mL/min
- DSC 823 test n°: 2693
The heat flow record shows an endothermic effect between 157 °C and 310 °C, with peak at 274 °C and onset at 265 °C.
The boiling temperature of the sample labelled as 2E4MZ-CN is 265 °C (first test).
Second test:
- sample amount: 6.61 mg
- crucible: Aluminum, lid with a 50 μm hole
- heating rate: 5 °C/min
- temperature range: 30-500 °C
- atmosphere: N2 flow, 20 mL/min
- DSC 823 test n°: 2695
The heat flow record shows an endothermic effect between 159 °C and 319 °C, with peak at 275 °C and onset at 265 °C.
The boiling temperature of the sample labelled as 2E4MZ-CN is 265 °C (second test).
The initial boiling temperature of the sample labelled as 2E4MZ-CN is 265 °C (the mean of two measurements).
Applicant's summary and conclusion
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