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Please be aware that this old REACH registration data factsheet is no longer maintained; it remains frozen as of 19th May 2023.

The new ECHA CHEM database has been released by ECHA, and it now contains all REACH registration data. There are more details on the transition of ECHA's published data to ECHA CHEM here.

Diss Factsheets

Physical & Chemical properties

Particle size distribution (Granulometry)

Administrative data

Endpoint:
particle size distribution (granulometry)
Type of information:
experimental study
Adequacy of study:
key study
Reliability:
1 (reliable without restriction)
Rationale for reliability incl. deficiencies:
guideline study

Data source

Reference
Reference Type:
study report
Title:
Unnamed
Year:
2017
Report date:
2017

Materials and methods

Test guidelineopen allclose all
Qualifier:
according to guideline
Guideline:
ISO 13320 (Particle size analysis - Laser diffraction methods)
Deviations:
no
Qualifier:
according to guideline
Guideline:
other: CIPAC MT 187.
Deviations:
no
GLP compliance:
yes (incl. QA statement)
Type of method:
Laser scattering/diffraction
Type of particle tested:
primary particle
Type of distribution:
mass based distribution

Test material

Constituent 1
Reference substance name:
Reaction products of diazotized 4-amino-6-[(4-aminophenyl)diazenyl]-3-[(4-aminophenyl)diazenyl]-5-hydroxynaphthalene-2,7-disulfonic acid, coupled with benzene-1,3-diamine, sodium salts
EC Number:
812-037-7
Cas Number:
1793011-72-9
Molecular formula:
Unknown for all components
IUPAC Name:
Reaction products of diazotized 4-amino-6-[(4-aminophenyl)diazenyl]-3-[(4-aminophenyl)diazenyl]-5-hydroxynaphthalene-2,7-disulfonic acid, coupled with benzene-1,3-diamine, sodium salts
Test material form:
solid

Results and discussion

Mass median aerodynamic diameter:
194.091 µm
Geometric standard deviation:
>= 2.85 - <= 2.884
Particle sizeopen allclose all
Percentile:
D10
Mean:
39.793 µm
St. dev.:
0.319
Percentile:
D50
Mean:
153.442 µm
St. dev.:
2.03
Percentile:
D90
Mean:
428.178 µm
St. dev.:
9.999

Any other information on results incl. tables

Visually the sample was observed to be a black powder with clusters. Using a 3.2 objective lens the particles appeared to be irregular shaped crystals. The smallest individual particle size was approximately 10 μm and the largest individual size was approximately 432 μm. Using a 40 objective lens the sample was observed to be made up of single crystalline particles.

Applicant's summary and conclusion

Conclusions:
The particle size mass median aerodynamic diameter (MMAD) was determined to be 194.091 µm and the volume of sample with particles < 10 µm was 0.63%.