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Please be aware that this old REACH registration data factsheet is no longer maintained; it remains frozen as of 19th May 2023.

The new ECHA CHEM database has been released by ECHA, and it now contains all REACH registration data. There are more details on the transition of ECHA's published data to ECHA CHEM here.

Diss Factsheets

Administrative data

Endpoint:
melting point/freezing point
Type of information:
experimental study
Adequacy of study:
key study
Study period:
03 - 13 July 2009
Reliability:
2 (reliable with restrictions)
Rationale for reliability incl. deficiencies:
other: Valid method similar to OECD guideline and EU test method

Data source

Reference
Reference Type:
study report
Title:
Unnamed
Year:
2009
Report date:
2009

Materials and methods

Test guidelineopen allclose all
Qualifier:
equivalent or similar to guideline
Guideline:
EU Method A.1 (Melting / Freezing Temperature)
Qualifier:
equivalent or similar to guideline
Guideline:
OECD Guideline 102 (Melting point / Melting Range)
Type of method:
thermal analysis

Test material

Constituent 1
Chemical structure
Reference substance name:
Butanamide, 2,2'-[(3,3'-dichloro[1,1'-biphenyl]-4,4'-diyl)bis(azo)]bis[3-oxo-, N,N'-bis(phenyl and o-tolyl) derivs.
EC Number:
272-732-0
EC Name:
Butanamide, 2,2'-[(3,3'-dichloro[1,1'-biphenyl]-4,4'-diyl)bis(azo)]bis[3-oxo-, N,N'-bis(phenyl and o-tolyl) derivs.
Cas Number:
68910-13-4
Molecular formula:
C32H26O4N6Cl2 - C34H30O4N6Cl2
IUPAC Name:
Reaction mass of 2,2'-[(3,3'-dichloro[1,1'-biphenyl]-4,4'-diyl)bis(2,1-diazendiyl)]bis[3-oxo-N-phenylbutyramide], 2,2'-[(3,3'-dichloro[1,1'-biphenyl]-4,4'-diyl)bis(2,1-diazenediyl)]bis[N-(2-methylphenyl)-3-oxobutyramide] and 2-[2-[3,3'-dichloro-4'-[2-[1-[[(2-methylphenyl)amino]carbonyl]-2-oxopropyl]diazenyl][1,1'-biphenyl]-4-yl]diazenyl]-3-oxo-N-phenylbutyramide

Results and discussion

Melting / freezing point
Melting / freezing pt.:
°C
Decomposition:
yes
Decomp. temp.:
> 300 °C

Any other information on results incl. tables

No melting point could be determined. The TGA points to decomposition well above 300 °C.

Applicant's summary and conclusion

Conclusions:
The decomposition temperature of the test substance is above 300 °C.
Executive summary:

When tested in a study using methods based on OECD guidelines and EU test methods, the test substance showed no melting point up to 300°C withdecomposition taking place well above 300°C.