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Boiling point

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Reference
Endpoint:
boiling point
Type of information:
experimental study
Adequacy of study:
key study
Study period:
2014-09-29 to 2014-10-01
Reliability:
1 (reliable without restriction)
Rationale for reliability incl. deficiencies:
guideline study
Reason / purpose for cross-reference:
reference to same study
Qualifier:
according to guideline
Guideline:
EU Method A.2 (Boiling Temperature)
Deviations:
no
Qualifier:
according to guideline
Guideline:
OECD Guideline 103 (Boiling point/boiling range)
Version / remarks:
(1995)
Deviations:
no
GLP compliance:
no
Type of method:
differential scanning calorimetry
Key result
Boiling pt.:
135.3 °C
Atm. press.:
1 013 hPa
Decomposition:
no

Results of the DSC measurements

Measurement No.

Onset of Effect\°C

Range of effect\°C

Atmospheric pressure\hPa

1

135.31

100-180 (endo)

1010.9

2

135.14

100-160 (endo)

1012.7

During the heating phase the test item showed an endothermic signal in the temperature range of approx. 100 - 180°C that can be associated with the boiling of the test item. The lowest measured onset temperature is corrected to the standard pressure to be 135.16 °C and the highest onset temperature to be 135.39 °C. As the corrected onset temperatures in both tests deviate by less than 0.5 K from their mean value of 135.28 °C, the test item has a boiling point of 135.3 °C. No further thermal effects were observed up to the maximum test temperature of 500°C.

Conclusions:
The test item has a boiling point of 135.3 °C corrected to normal atmospheric pressure (1013 hPa) as determined by differential scanning calorimetry according to Regulation EC No. 440/2008 Method A.2., OECD Test Guideline 103 (1995)..

Description of key information

Boiling point: 135.3 °C at 1013 hPa

Key value for chemical safety assessment

Boiling point at 101 325 Pa:
135.3 °C

Additional information

The test item has a boiling point of 135.3 °C corrected to normal atmospheric pressure (1013 hPa) as determined by differential scanning calorimetry according to Regulation EC No. 440/2008 Method A.2., OECD Test Guideline 103 (1995).