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Diss Factsheets

Physical & Chemical properties

Melting point / freezing point

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Administrative data

Link to relevant study record(s)

Reference
Endpoint:
melting point/freezing point
Type of information:
experimental study
Adequacy of study:
key study
Reliability:
1 (reliable without restriction)
Rationale for reliability incl. deficiencies:
guideline study
Reason / purpose for cross-reference:
reference to same study
Reason / purpose for cross-reference:
reference to same study
Qualifier:
according to guideline
Guideline:
OECD Guideline 102 (Melting point / Melting Range)
Qualifier:
according to guideline
Guideline:
EU Method A.1 (Melting / Freezing Temperature)
GLP compliance:
no
Type of method:
differential scanning calorimetry
Key result
Melting / freezing pt.:
56.5 °C
Atm. press.:
1 005 hPa
Decomposition:
no
Sublimation:
no
Remarks on result:
other: Mean value of 2 replicate measurements

During the heating phase, an endothermal effect was observed in the temperature range of 50 to 70 °C, which can be assigned to the melting of the test item.

The results of the 2 replicate measurements are:

Replicate

sample weight (mg)

Onset of effect (°C)

Range of effect (°C)

Atmospheric pressure (hPa)

1

8.99

56.48

50 to 70 (endo)

1005.2

2

10.87

56.59

50 to 70 (endo)

1005.2

As the onset temperatures in both tests deviate less than 0.5 K from their mean value of 56.54 °C, the mean value is used as melting point.

 

Conclusions:
The test item has a melting point of 56.5 °C at atmospheric pressure (1005hPa).
Executive summary:

The melting point of the test item was assessed according to OECD 102, differential scanning calorimetry. The measurement was performed in duplicate. An endothermic effect was observed in the range of 50 to 70°C. The mean melting point temperature was derived to be 56.5°C at atmospheric pressure (1005 hPa).

Description of key information

The test item has a melting point of 56.5 °C at atmospheric pressure, as determined according to OECD 102, differential scanning calorimetry.

Key value for chemical safety assessment

Melting / freezing point at 101 325 Pa:
56.5 °C

Additional information

In a recent study the melting temperature of the test item was determined according to the OECD 102 by differential scanning calorimetry. A thermogram is obtained in which the transition heat flow is exhibited as function of the temperature. In this diagram, the onset of the process as well as the heat flow of the process are shown.

The test item has a melting point of 56.5 °C at atmospheric pressure.