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Diss Factsheets

Physical & Chemical properties

Boiling point

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Administrative data

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Reference
Endpoint:
boiling point
Type of information:
experimental study
Adequacy of study:
key study
Study period:
04 February 2016 - 20 June 2016
Reliability:
1 (reliable without restriction)
Rationale for reliability incl. deficiencies:
guideline study
Qualifier:
according to guideline
Guideline:
EU Method A.2 (Boiling Temperature)
Deviations:
no
Qualifier:
according to guideline
Guideline:
OECD Guideline 103 (Boiling Point)
Version / remarks:
1995
Deviations:
no
GLP compliance:
no
Remarks:
Study was not performed under GLP, however the test facility was GLP-compliant.
Type of method:
differential scanning calorimetry
Key result
Boiling pt.:
>= 262 - <= 264 °C
Atm. press.:
1 013 hPa

The test item showed an endothermic signal in the temperature range of approximately 150 – 290°C that can be assigned to the boiling of the test item. For the correction of the boiling temperature to standard pressure the test item was assigned to chemical group 3 (e.g. esters). A correction value φ = 5.3 was used for the temperature of 260 – 270°C, according to Hass and Newton. The lowest measured onset temperature is corrected to the standard pressure to be 261.86°C and the highest onset temperature to be 264.21°C. As the corrected onset temperatures in both tests deviate by more than 0.5 K from their mean value of 263.04°C, the test item has a boiling range of 262 – 264°C. No further thermal effects were observed up to the maximum test temperature of 500°C.

Conclusions:
The boiling point of the test item was determined to be 262 to 264°C at atmospheric pressure.
Executive summary:

Boiling point was determined by differential scanning calorimetry according to OECD Guideline 103 and EU Method A.2. The boiling point of the test item was determined to be 262 to 264°C at atmospheric pressure. The study was not performed under GLP, however the test facility was GLP-compliant. The study is considered to be reliable without restrictions (Klimisch 1).

Description of key information

The boiling point of the test item was determined to be 262 to 264°C at atmospheric pressure.

Key value for chemical safety assessment

Boiling point at 101 325 Pa:
262 °C

Additional information

Boiling point was determined by differential scanning calorimetry according to OECD Guideline 103 and EU Method A.2. The study was not performed under GLP, however the test facility was GLP-compliant. The study is considered to be reliable without restrictions (Klimisch 1).