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Please be aware that this old REACH registration data factsheet is no longer maintained; it remains frozen as of 19th May 2023.

The new ECHA CHEM database has been released by ECHA, and it now contains all REACH registration data. There are more details on the transition of ECHA's published data to ECHA CHEM here.

Diss Factsheets

Physical & Chemical properties

Boiling point

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Administrative data

Link to relevant study record(s)

Reference
Endpoint:
boiling point
Type of information:
experimental study
Adequacy of study:
key study
Study period:
2014
Reliability:
1 (reliable without restriction)
Rationale for reliability incl. deficiencies:
guideline study
Qualifier:
according to guideline
Guideline:
OECD Guideline 103 (Boiling Point/Boiling Range)
Qualifier:
according to guideline
Guideline:
EU Method A.2 (Boiling Temperature)
GLP compliance:
no
Type of method:
differential scanning calorimetry
Key result
Atm. press.:
ca. 1 013 hPa
Decomposition:
yes
Remarks:
Test item decomposed prior to boiling
Decomp. temp.:
>= 320 - <= 345 °C

DSC measurements in aluminium crucibles with a hole showed an endothermal effect in the temperature range of 150 -225°C with onset temperatures between 206.12°C and 211.83°C. A second endothermal effect was observed in the temperature range of 320 -345°C with an unsteady onset. From the results of DSC measurements it was concluded that the test item had a melting range of 206 -212°C. The second endothermal effect in the temperature range 320 -345°C was not interpreted as boiling since approx. 50% of the test item mass remain as black residue and the DSC-measurement in a closed glass crucible showed an exothermal signal in the temperature range of 280°C and 350°C. It was concluded that the test item had no boiling point. The test item decomposed prior to boiling.

Description of key information

The test item had no boiling point. The test item decomposed prior to boiling.

Key value for chemical safety assessment

Additional information