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Diss Factsheets

Administrative data

Endpoint:
water solubility
Type of information:
experimental study
Adequacy of study:
key study
Study period:
15 Jul - 12 Oct 2016
Reliability:
1 (reliable without restriction)
Rationale for reliability incl. deficiencies:
guideline study

Data source

Reference
Reference Type:
study report
Title:
Unnamed
Year:
2016
Report date:
2016

Materials and methods

Test guideline
Qualifier:
according to guideline
Guideline:
EU Method A.6 (Water Solubility)
GLP compliance:
no
Type of method:
flask method

Test material

Constituent 1
Reference substance name:
Reaction mass of ammonium dodecyl sulfate, ammonium tetradecyl sulfate and ammonium alkoxy-alkyl sulfate
Molecular formula:
n.a. (UVCB substance)
IUPAC Name:
Reaction mass of ammonium dodecyl sulfate, ammonium tetradecyl sulfate and ammonium alkoxy-alkyl sulfate
Test material form:
solid

Results and discussion

Water solubility
Key result
Water solubility:
9.8 g/L
Temp.:
20 °C
pH:
>= 4.41 - <= 4.44
Remarks on result:
other: standard deviation ±0.558 g/L

Any other information on results incl. tables

Preliminary test:

Different amounts of the test item were suspended in deionised water and the respective mixture was stirred 2h at room temperature. The results are summarized below. As they were above 0.01 g/L, the flask method was selected.

Experiment

Water [mL]

Weighed Sample [g]

Result

A

2.0

2.6

cloudy liquid

B

6.5

1.5

clear liquid

C

2.0

16.8

cloudy liquid

D

2.3

65.9

cloudy liquid

E

2.5

132.0

cloudy liquid

Main test

The results are summarized in the table below:

Incubation time [h]

Individual results [mg/25 mL]

Average water solubility [g/L]

24

264.51/255.732

10.40

48

243.037/246.647

9.79

72

233.755/226.422

9.20

The test solutions were slightly hazy; this likely results in a slight overestimation of the water solubility.

The pH value of the sample solution was 4.44 (4.41, 4.42) after 24 (48, 72) hours of incubation.

Applicant's summary and conclusion

Conclusions:
Interpretation of results: miscible