Registration Dossier

Administrative data

Endpoint:
boiling point
Type of information:
experimental study
Adequacy of study:
key study
Study period:
2016
Reliability:
1 (reliable without restriction)
Rationale for reliability incl. deficiencies:
guideline study
Cross-reference
Reason / purpose for cross-reference:
reference to same study
Remarks:
4.2

Data source

Reference
Reference Type:
study report
Title:
Unnamed
Year:
2016
Report date:
2016

Materials and methods

Test guidelineopen allclose all
Qualifier:
according to guideline
Guideline:
OECD Guideline 103 (Boiling Point)
Deviations:
no
Qualifier:
according to guideline
Guideline:
EU Method A.2 (Boiling Temperature)
Deviations:
no
GLP compliance:
yes
Other quality assurance:
other: quality assurance statement
Type of method:
differential scanning calorimetry

Test material

Constituent 1
Reference substance name:
Rye, ext.
EC Number:
290-271-3
EC Name:
Rye, ext.
Cas Number:
90106-48-2
IUPAC Name:
Oligosaccharides and polysaccharides of glucose from Rye
Test material form:
solid: particulate/powder
Details on test material:
- Appearance: white powder
- Storage In darkness at room temperature
- Batch: 16 167
- Manufacturing date: June 2016
- Expiry date: June 2018

Results and discussion

Boiling point
Key result
Atm. press.:
>= 101 320 - <= 101 330 Pa
Decomposition:
yes
Remarks:
At about 200°C, the test item aspect changed, the powder inflated and then a decomposition was observed
Decomp. temp.:
ca. 200 °C
Remarks on result:
other: No boiling point was recorded

Any other information on results incl. tables

essai 1 : an evaporation of the hydration water was recorded from about 47°C to about 110 -120°C. No boiling point of the test item was recorded.

essai 2 : the evaporation of the hydratation water was confirmed from about 47°C to about 120°C. No boiling point of the test item was recorded.

A complementary assay was carried out with a Köfler bench to confirm the decomposition of the test item. A small quantity of the test item was put on the hot surface at different temperatures. At about 150 °C, the colour of the powder became darker. At about 200 °C, the test item aspect changed, the powder inflated and then a decomposition was observed.

Applicant's summary and conclusion

Conclusions:
An evaporation of the hydration water was recorded from about 50°C to about 100°C. No boiling point of the test item was recorded.
Executive summary:

The boiling point of the test substance was tested under GLP according to EU A2 and OECD 103, by differential scanning calorimetry. Three runs were performed under nitrogen atmosphere, and one complementary assa ywas carried out with a Köfler bench to confirm the decomposition of the test item and no boiling point was recorded.

The test item inflated and darkened sign of decomposition.