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Please be aware that this old REACH registration data factsheet is no longer maintained; it remains frozen as of 19th May 2023.

The new ECHA CHEM database has been released by ECHA, and it now contains all REACH registration data. There are more details on the transition of ECHA's published data to ECHA CHEM here.

Diss Factsheets

Physical & Chemical properties

Particle size distribution (Granulometry)

Administrative data

Endpoint:
particle size distribution (granulometry)
Type of information:
experimental study
Adequacy of study:
key study
Study period:
2020
Reliability:
1 (reliable without restriction)
Rationale for reliability incl. deficiencies:
guideline study

Data source

Reference
Reference Type:
study report
Title:
Unnamed
Year:
2020
Report date:
2020

Materials and methods

Test guideline
Qualifier:
equivalent or similar to guideline
Guideline:
ISO 13320 (Particle size analysis - Laser diffraction methods)
GLP compliance:
yes (incl. QA statement)
Remarks:
Hessisches Ministerium für Umwelt, Klimaschutz, Landwirtschaft und Verbraucherschutz
Type of method:
Laser scattering/diffraction
Type of distribution:
volumetric distribution

Test material

Constituent 1
Chemical structure
Reference substance name:
3-(difluoromethyl)-1-methyl-1H-pyrazole-4-carboxylic acid
EC Number:
700-093-4
Cas Number:
176969-34-9
Molecular formula:
C6H6F2N2O2
IUPAC Name:
3-(difluoromethyl)-1-methyl-1H-pyrazole-4-carboxylic acid

Results and discussion

Particle sizeopen allclose all
Percentile:
D10
Mean:
10.7 µm
Remarks on result:
other: St. dev. not reported
Percentile:
D50
Mean:
35.6 µm
Remarks on result:
other: St. dev. not reported
Percentile:
D90
Mean:
78.5 µm
Remarks on result:
other: St. dev. not reported

Any other information on results incl. tables

The median particle size L50 (D (v, 0.5): 50 % of particle volume with lower particle diameter) deduced from these distributions were:

1st test series: L50 = 35.1 µm

2nd test series: L50 = 36.0 µm

The average of the median particle size L50 was:

L50 35.6 µm

The particle size L10 (D (v, O. 1): 10 % of particle volume with lower particle diameter) deduced from these distributions were:

1st test series: L10 = 10.5 µm

2nd test series: L10 = 10.8 µm

The average of the particle size L10 was:

L10 = 10.7 µm

The particle size L90 (D (v, 0.9): 90 % of particle volume with lower particle diameter) deduced from these distributions were:

1st test series: L90 = 77.6 µm

2nd test series: L90 = 79.5 µm

The average of the particle size L90 was:

L90 = 78.5 µm

Two maxima were observed at approximately 1-2 µm and approximately 40 µm.

Applicant's summary and conclusion