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Please be aware that this old REACH registration data factsheet is no longer maintained; it remains frozen as of 19th May 2023.

The new ECHA CHEM database has been released by ECHA, and it now contains all REACH registration data. There are more details on the transition of ECHA's published data to ECHA CHEM here.

Diss Factsheets

Administrative data

Endpoint:
boiling point
Type of information:
experimental study
Adequacy of study:
key study
Study period:
2009
Reliability:
1 (reliable without restriction)

Data source

Reference
Reference Type:
study report
Title:
Unnamed
Year:
2009
Report date:
2009

Materials and methods

Test guideline
Qualifier:
according to guideline
Guideline:
other: DSC method
Deviations:
not applicable
Principles of method if other than guideline:
Equipment: Mettler Toledo DSC 823e
Standard Operating Procedure: AA 1020-2007 + AA 1020-1128
Temp. range 25 °C up to 300 °C, heating rate: 10 K/min
measured in Aluminium pan with hole (50 µm)
Peak: 264 °C
Onset: 250 °C
In accordance with procedure AA 1020-1128, the boiling point is taken as the mean of peak and onset
GLP compliance:
not specified
Type of method:
other: Differential Scanning Calorimetry

Test material

Constituent 1
Chemical structure
Reference substance name:
2'-methoxyacetoacetanilide
EC Number:
202-131-0
EC Name:
2'-methoxyacetoacetanilide
Cas Number:
92-15-9
Molecular formula:
C11H13NO3
IUPAC Name:
N-(2-methoxyphenyl)-3-oxobutanamide

Results and discussion

Boiling point
Boiling pt.:
257 °C
Atm. press.:
ca. 1 atm
Decomposition:
no
Decomp. temp.:
> 450 °C

Applicant's summary and conclusion

Executive summary:

The boiling point of the test item determined by DSC is 257°C