Registration Dossier

Diss Factsheets

Administrative data

Endpoint:
boiling point
Type of information:
experimental study
Adequacy of study:
key study
Study period:
2009
Reliability:
1 (reliable without restriction)

Data source

Reference
Reference Type:
study report
Title:
Unnamed
Year:
2009
Report date:
2009

Materials and methods

Test guideline
Qualifier:
according to guideline
Guideline:
other: DSC method
Deviations:
not applicable
Principles of method if other than guideline:
Equipment: Mettler Toledo DSC 823e
Standard Operating Procedure: AA 1020-2007 + AA 1020-1128
Temp. range 25 °C up to 300 °C, heating rate: 10 K/min
measured in Aluminium pan with hole (50 µm)
Peak: 264 °C
Onset: 250 °C
In accordance with procedure AA 1020-1128, the boiling point is taken as the mean of peak and onset
GLP compliance:
not specified
Type of method:
other: Differential Scanning Calorimetry

Test material

Constituent 1
Chemical structure
Reference substance name:
2'-methoxyacetoacetanilide
EC Number:
202-131-0
EC Name:
2'-methoxyacetoacetanilide
Cas Number:
92-15-9
Molecular formula:
C11H13NO3
IUPAC Name:
N-(2-methoxyphenyl)-3-oxobutanamide

Results and discussion

Boiling point
Boiling pt.:
257 °C
Atm. press.:
ca. 1 atm
Decomposition:
no
Decomp. temp.:
> 450 °C

Applicant's summary and conclusion

Executive summary:

The boiling point of the test item determined by DSC is 257°C