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Melting point / freezing point

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Reference
Endpoint:
melting point/freezing point
Type of information:
experimental study
Adequacy of study:
key study
Study period:
21-07-2011
Reliability:
1 (reliable without restriction)
Rationale for reliability incl. deficiencies:
guideline study
Qualifier:
according to guideline
Guideline:
EU Method A.1 (Melting / Freezing Temperature)
Deviations:
no
GLP compliance:
yes (incl. QA statement)
Type of method:
method to determine freezing temperature
Specific details on test material used for the study:
- Name of test material (as cited in study report): MOPA, 3-methoxypropylamine
- Physical state: Liquid
- Analytical urity: 99.4% by GC
- Purity test date: 12-04-2010
- Lot/batch No.: 9M603
Key result
Melting / freezing pt.:
< -20 °C
Decomposition:
no
Sublimation:
no
Remarks on result:
other: Atmospheric pressure not reported; ambient conditions are anticipated

In both runs no crystallisation was observed down to -25°C, therefore the test was terminated.

Conclusions:
The freezing temperature of the substance was concluded to be below -20°C under ambient conditions.

Description of key information

The freezing point of the test substance under ambient conditions was determined to be below -20°C in a GLP study according to test method EC A.1 (Shajad Younis, 2011).

Key value for chemical safety assessment

Additional information

The freezing point of the test item was determined to be <-20°C.