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Diss Factsheets

Physical & Chemical properties

Boiling point

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Administrative data

Link to relevant study record(s)

Reference
Endpoint:
boiling point
Type of information:
experimental study
Adequacy of study:
key study
Reliability:
1 (reliable without restriction)
Rationale for reliability incl. deficiencies:
guideline study
Qualifier:
according to guideline
Guideline:
EU Method A.2 (Boiling Temperature)
Version / remarks:
(December 1992)
Deviations:
no
Qualifier:
according to guideline
Guideline:
OECD Guideline 103 (Boiling point/boiling range)
Version / remarks:
(27 July 1995)
Deviations:
no
GLP compliance:
yes (incl. QA statement)
Type of method:
differential scanning calorimetry
Specific details on test material used for the study:
- Name of test material: Fatty acids, C16-18, reaction products with tetraethylenepentamine, acetates (salts)
Key result
Boiling pt.:
>= 390 °C
Decomposition:
yes
Decomp. temp.:
>= 390 °C

Using thermal analysis, no endothermic peaks were detected in the temperature range between 25 °C and 400 °C from which boiling could be deduced.

A second DSC run was performed in the same temperature range (25 °C to 400 °C) but with the temperature rise adjusted to 10 K/min. At about 390 °C an exothermic heat effect was observed, After the experiment the test item was dark brown and molten and had lost about 41 % of its mass.

In conclusion, decomposition was observed before boiling occurred.

Conclusions:
No boiling point was detected for C1618FA-TEPA-compound prior to decomposition.
Executive summary:

The boiling point of C16 18FA-TEPA-compound was determined according to EU method A.2, December 1992 and OECD guideline 103, 27 July 1995 (differential scanning calorimetry). No boiling point was detected prior to decomposition.

Description of key information

No boiling point was detected prior to decomposition (EU method A.2/OECD guideline 103; differential scanning calorimetry).

Key value for chemical safety assessment

Temperature of decomposition (state purity):
390 °C

Additional information

The boiling point of C16 18FA-TEPA-compound was determined according to EU method A.2, December 1992 and OECD guideline 103, 27 July 1995 (differential scanning calorimetry). No boiling point was detected prior to decomposition.