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EC number: 422-150-1 | CAS number: -
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- Ecotoxicological Summary
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- Toxicological Summary
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- Acute Toxicity
- Irritation / corrosion
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Endpoint summary
Administrative data
Description of key information
Alcamizer 5 was tested in two adjuvant type guinea pig test method for
skin sensitisation according to OECD 406 guideline and GLP principles.
The results of the first study lead to a sensitisation rate of 20% and
in the second test none of the ten experimental animals showed positive
reactions during challenge with Alcamizer 5.
Key value for chemical safety assessment
Skin sensitisation
Link to relevant study records
- Endpoint:
- skin sensitisation: in vivo (non-LLNA)
- Type of information:
- experimental study
- Adequacy of study:
- key study
- Study period:
- 04 April, 1995 - 05 May, 1995
- Reliability:
- 1 (reliable without restriction)
- Rationale for reliability incl. deficiencies:
- guideline study
- Qualifier:
- according to guideline
- Guideline:
- OECD Guideline 406 (Skin Sensitisation)
- Version / remarks:
- (1992)
- Deviations:
- no
- Qualifier:
- according to guideline
- Guideline:
- EU Method B.6 (Skin Sensitisation)
- Version / remarks:
- (1992)
- Deviations:
- no
- Qualifier:
- according to guideline
- Guideline:
- other: "Allergic Contact Dermatitis in the Guinea-Pig: Identification of Contact Allergens" Magnusson B. Kligman A.M., 1970 published by C.C. Thomas, Springfield, Illinois, USA.
- GLP compliance:
- yes
- Type of study:
- guinea pig maximisation test
- Justification for non-LLNA method:
- Adequate data from a reliable GPMT study were already available.
- Species:
- guinea pig
- Strain:
- Dunkin-Hartley
- Sex:
- female
- Details on test animals and environmental conditions:
- TEST ANIMALS
- Source: Charles River, Germany
- Age at study initiation: approx. 6-7 weeks
- Weight at study initiation: 446-556 g
- Housing: Group housing of 2 animals, except for 1 control animal, per labelled metal cage with wire-mesh floors.
- Diet: Free access to standard guinea pig diet, including ascorbic acid (1600 mg/kg) (LC 23-B, pellet diameter 4mm, Hope Farms, Woerden, The Netherlands)
- Water: Free access to tap water, diluted with decalcified water.
- Acclimation period: At least 5 days
ENVIRONMENTAL CONDITIONS
- Temperature (°C): 21
- Humidity (%): 50
- Air changes (per hr): approx. 15
- Photoperiod (hrs dark / hrs light): 12/12 - Route:
- intradermal and epicutaneous
- Vehicle:
- other: distilled water
- Concentration / amount:
- - 25% for the intradermal induction
- 50% for the epidermal induction
- 0, 10, 25 and 50% for the challenge - Route:
- epicutaneous, occlusive
- Vehicle:
- other: distilled water
- Concentration / amount:
- - 25% for the intradermal induction
- 50% for the epidermal induction
- 0, 10, 25 and 50% for the challenge - No. of animals per dose:
- Number of animals in test group: 10
Number of animals in negative control group: 5 - Details on study design:
- RANGE FINDING TESTS (4 animals, age: approx. 6-7 weeks)
For the intradermal induction exposure (2 animals):
- Concentration: 10 and 25%; and 2 and 5%
- Amounts: 0.1 mL. Each of the 2 animals received 2 different concentrations in the right and left clipped shoulder regions.
- Scoring: the skin reactions were scored 24 and 48 hours after application
For the epicutaneous induction, using Scotchpak-non-woven patch (the same animals as above):
- Concentration: 50 and 25%
- Amount: 0.5 mL. Each of the 2 animals received a differerent concentration to the shaved flank of the animal.
- Exposure period: 24 hours (occlusive)
- Scoring: the skin reactions were scored 24 and 48 hours after patch removal
For the epicutaneous induction, using square chambers (2 animals):
- Concentration: 50, 25, 10 and 5%
- Amount: 0.05 mL were applied occlusively on a shaved flank of each of the 2 animals.
- Exposure period: 24 hours (occlusive)
- Scoring: the skin reactions were scored 24 and 48 hours after patch removal
MAIN STUDY
Test animals: 10
Control animals: 5
A. INDUCTION EXPOSURE
- No. of exposures: 2
1) Intradermal injections on day 1:
- Concentration: 25%
- Site: clipped scapular region. One of each pair was on each side of the midline and from cranial A) to caudal C):
Three pairs of intradermal injections:
1) 0.1 mL: FCA (50% in water)
2) 0.1 mL: test substance at a 25% concentration in distilled water (control animals: 0.1 mL distilled water)
3) 0.1 mL: 50% test substance in distilled water + 50% FCA (undiluted) (control animals: 50% with distilled water + 50% FCA (undiluted))
-Readings: on day 3 (48 hrs after the injections). Irritating results were observed in the test groups, in each of the 3 sites.
- Use of SDS (all animals): on day 8, 24 hrs before the topical induction application, the scapular area was clipped and subsequently rubbed with 10% SDS in vaseline using a spatula.
2)Topical application on day 9:
- Concentration: 50%
- Amount: 0.5 mL (control animals: 0.5 mL of distilled water), on the SDS treated area
- Exposure period: 48 hours (occlusive)
- Readings: scores were rated directly after patch removal (skin cleaned of residual test substance)
B. CHALLENGE EXPOSURE (all animals)
- Concentration: 0, 10, 25 and 50%
- Day of challenge: day 22 (13 days after the start of the 2nd induction)
- Exposure period: 24 hours (occlusive)
- Site: flank
- Amount: 0.5 mL
- Readings: scores were rated 24 and 48 hours after patch removal - Challenge controls:
- Not applicable.
- Positive control substance(s):
- yes
- Remarks:
- (the results of the latest reliability check, performed in December 1994 with Alpha-hexylcinnamicaldehyde, tech. 85%, are reported)
- Positive control results:
- The latest reliability check (performed less than 6 months ago) shows a sensitisation rate of 90%. See the attached background material.
- Reading:
- 1st reading
- Hours after challenge:
- 24
- Group:
- test chemical
- Dose level:
- 50 %
- No. with + reactions:
- 0
- Total no. in group:
- 10
- Remarks on result:
- other: Reading: 1st reading. . Hours after challenge: 24.0. Group: test group. Dose level: 50 %. No with. + reactions: 0.0. Total no. in groups: 10.0.
- Reading:
- 1st reading
- Hours after challenge:
- 24
- Group:
- test chemical
- Dose level:
- 25 %
- No. with + reactions:
- 0
- Total no. in group:
- 10
- Remarks on result:
- other: Reading: 1st reading. . Hours after challenge: 24.0. Group: test group. Dose level: 25 %. No with. + reactions: 0.0. Total no. in groups: 10.0.
- Reading:
- 1st reading
- Hours after challenge:
- 24
- Group:
- test chemical
- Dose level:
- 10 %
- No. with + reactions:
- 0
- Total no. in group:
- 10
- Remarks on result:
- other: Reading: 1st reading. . Hours after challenge: 24.0. Group: test group. Dose level: 10 %. No with. + reactions: 0.0. Total no. in groups: 10.0.
- Reading:
- 1st reading
- Hours after challenge:
- 24
- Group:
- test chemical
- Dose level:
- 0 %
- No. with + reactions:
- 0
- Total no. in group:
- 10
- Remarks on result:
- other: Reading: 1st reading. . Hours after challenge: 24.0. Group: test group. Dose level: 0 %. No with. + reactions: 0.0. Total no. in groups: 10.0.
- Reading:
- 2nd reading
- Hours after challenge:
- 48
- Group:
- test chemical
- Dose level:
- 50 %
- No. with + reactions:
- 2
- Total no. in group:
- 10
- Remarks on result:
- other: Reading: 2nd reading. . Hours after challenge: 48.0. Group: test group. Dose level: 50 %. No with. + reactions: 2.0. Total no. in groups: 10.0.
- Reading:
- 2nd reading
- Hours after challenge:
- 48
- Group:
- test chemical
- Dose level:
- 25 %
- No. with + reactions:
- 2
- Total no. in group:
- 10
- Remarks on result:
- other: Reading: 2nd reading. . Hours after challenge: 48.0. Group: test group. Dose level: 25 %. No with. + reactions: 2.0. Total no. in groups: 10.0.
- Reading:
- 2nd reading
- Hours after challenge:
- 48
- Group:
- test chemical
- Dose level:
- 10 %
- No. with + reactions:
- 2
- Total no. in group:
- 10
- Remarks on result:
- other: Reading: 2nd reading. . Hours after challenge: 48.0. Group: test group. Dose level: 10 %. No with. + reactions: 2.0. Total no. in groups: 10.0.
- Reading:
- 2nd reading
- Hours after challenge:
- 48
- Group:
- test chemical
- Dose level:
- 0 %
- No. with + reactions:
- 0
- Total no. in group:
- 10
- Remarks on result:
- other: Reading: 2nd reading. . Hours after challenge: 48.0. Group: test group. Dose level: 0 %. No with. + reactions: 0.0. Total no. in groups: 10.0.
- Reading:
- 1st reading
- Hours after challenge:
- 24
- Group:
- negative control
- Dose level:
- 50 %
- No. with + reactions:
- 0
- Total no. in group:
- 5
- Remarks on result:
- other: Reading: 1st reading. . Hours after challenge: 24.0. Group: negative control. Dose level: 50 %. No with. + reactions: 0.0. Total no. in groups: 5.0.
- Reading:
- 1st reading
- Hours after challenge:
- 24
- Group:
- negative control
- Dose level:
- 25 %
- No. with + reactions:
- 0
- Total no. in group:
- 5
- Remarks on result:
- other: Reading: 1st reading. . Hours after challenge: 24.0. Group: negative control. Dose level: 25 %. No with. + reactions: 0.0. Total no. in groups: 5.0.
- Reading:
- 1st reading
- Hours after challenge:
- 24
- Group:
- negative control
- Dose level:
- 10 %
- No. with + reactions:
- 0
- Total no. in group:
- 5
- Remarks on result:
- other: Reading: 1st reading. . Hours after challenge: 24.0. Group: negative control. Dose level: 10 %. No with. + reactions: 0.0. Total no. in groups: 5.0.
- Reading:
- 1st reading
- Hours after challenge:
- 24
- Group:
- negative control
- Dose level:
- 0 %
- No. with + reactions:
- 0
- Total no. in group:
- 5
- Remarks on result:
- other: Reading: 1st reading. . Hours after challenge: 24.0. Group: negative control. Dose level: 0 %. No with. + reactions: 0.0. Total no. in groups: 5.0.
- Reading:
- 2nd reading
- Hours after challenge:
- 48
- Group:
- negative control
- Dose level:
- 50 %
- No. with + reactions:
- 0
- Total no. in group:
- 5
- Remarks on result:
- other: Reading: 2nd reading. . Hours after challenge: 48.0. Group: negative control. Dose level: 50 %. No with. + reactions: 0.0. Total no. in groups: 5.0.
- Reading:
- 2nd reading
- Hours after challenge:
- 48
- Group:
- negative control
- Dose level:
- 25 %
- No. with + reactions:
- 0
- Total no. in group:
- 5
- Remarks on result:
- other: Reading: 2nd reading. . Hours after challenge: 48.0. Group: negative control. Dose level: 25 %. No with. + reactions: 0.0. Total no. in groups: 5.0.
- Reading:
- 2nd reading
- Hours after challenge:
- 48
- Group:
- negative control
- Dose level:
- 10 %
- No. with + reactions:
- 0
- Total no. in group:
- 5
- Remarks on result:
- other: Reading: 2nd reading. . Hours after challenge: 48.0. Group: negative control. Dose level: 10 %. No with. + reactions: 0.0. Total no. in groups: 5.0.
- Reading:
- 2nd reading
- Hours after challenge:
- 48
- Group:
- negative control
- Dose level:
- 0 %
- No. with + reactions:
- 0
- Total no. in group:
- 5
- Remarks on result:
- other: Reading: 2nd reading. . Hours after challenge: 48.0. Group: negative control. Dose level: 0 %. No with. + reactions: 0.0. Total no. in groups: 5.0.
- Reading:
- 1st reading
- Hours after challenge:
- 24
- Group:
- positive control
- Dose level:
- 10%, 25% and 50%
- No. with + reactions:
- 9
- Total no. in group:
- 10
- Remarks on result:
- positive indication of skin sensitisation
- Reading:
- 2nd reading
- Hours after challenge:
- 48
- Group:
- positive control
- Dose level:
- 10%, 25% and 50%
- No. with + reactions:
- 9
- Total no. in group:
- 10
- Remarks on result:
- positive indication of skin sensitisation
- Interpretation of results:
- other: not sensitising
- Remarks:
- According to Regulation (EC) No. 1272/2008 and its amendments.
- Conclusions:
- In an adjuvant type guinea pig test method for skin sensitisation according to OECD 406 guideline and GLP principles, two of the ten experimental animals showed positive reactions during challenge with Alcamizer 5.
- Executive summary:
Alcamizer 5 was tested in an adjuvant type guinea pig test method for skin sensitisation according to OECD 406 guideline and GLP principles.
After intradermal injection (sites without FCA) on day 3, moderate/severe erythema with or without necrosis was observed in all animals (experimental). On day 11, nine of the ten animals showed eschar formation and all ten animals showed moderate/severe erythema. Control animals showed no reactions. After epidermal application, nine of the ten experimental animals showed very slight to severe erythema. Two of the ten animals also showed eschar/crust formation. One of the five control animals showed very slight erythema.
One control animal died by accident on day 22. Pink discolouration of the lungs was found at post mortem macroscopic examination of this animal. No further mortality occurred and no symptoms of systemic toxicity were observed in the animals of the main study during the study period.
After the challenge, no skin reactions were evident after the challenge exposure.
Two animals showed discrete or patchy erythema in repsonse to the 50, 25 and 10% test substance concentrations 48 hours after patch removal. One other animal showed scaliness is response to the 50% concentration. These results lead to a sensitisation rate of 20%.
The latest reliability check (performed less than 6 months ago) shows a sensitisation rate of 90%.
- Endpoint:
- skin sensitisation: in vivo (non-LLNA)
- Type of information:
- experimental study
- Adequacy of study:
- key study
- Study period:
- 13 August, 1996 - 06 September, 1996
- Reliability:
- 1 (reliable without restriction)
- Rationale for reliability incl. deficiencies:
- guideline study
- Qualifier:
- according to guideline
- Guideline:
- OECD Guideline 406 (Skin Sensitisation)
- Version / remarks:
- (1992)
- Deviations:
- no
- Qualifier:
- according to guideline
- Guideline:
- EU Method B.6 (Skin Sensitisation)
- Version / remarks:
- (1992)
- Deviations:
- no
- Qualifier:
- according to guideline
- Guideline:
- other: "Allergic Contact Dermatitis in the Guinea-Pig: Identification of Contact Allergens" Magnusson B. Kligman A.M., 1970 published by C.C. Thomas, Springfield, Illinois, USA.
- GLP compliance:
- yes
- Type of study:
- guinea pig maximisation test
- Justification for non-LLNA method:
- Adequate data from a reliable GPMT study were already available.
- Species:
- guinea pig
- Strain:
- Himalayan
- Sex:
- female
- Details on test animals and environmental conditions:
- TEST ANIMALS
- Source: BRL Ltd., Basel, Switzerland
- Age at study initiation: approx. 5 weeks
- Weight at study initiation: 339-419 g
- Housing: Group housing of 5 animals per labelled metal cage with wire-mesh floors.
- Diet: Free access to standard guinea pig diet, including ascorbic acid (1600 mg/kg) (LC 23-B, pellet diameter 4mm, Hope Farms, Woerden, The Netherlands)
- Water: Free access to tap water, diluted with decalcified water.
- Acclimation period: At least 5 days
ENVIRONMENTAL CONDITIONS
- Temperature (°C): 21
- Humidity (%): 50
- Air changes (per hr): approx. 15
- Photoperiod (hrs dark / hrs light): 12/12 - Route:
- intradermal and epicutaneous
- Vehicle:
- other: distilled water
- Concentration / amount:
- - 25% for the intradermal induction
- 50% for the epidermal induction
- 0% and 50% for the challenge - Route:
- epicutaneous, occlusive
- Vehicle:
- other: distilled water
- Concentration / amount:
- - 25% for the intradermal induction
- 50% for the epidermal induction
- 0% and 50% for the challenge - No. of animals per dose:
- Number of animals in test group: 10
Number of animals in negative control group: 5 - Details on study design:
- RANGE FINDING TESTS (4 animals, age: approx. 6-7 weeks)
Selection of test substance concentrations for the main study were based on the preliminary irritation study of NOTOX project 137723 (see section 7.4.1) with the same test substance:
For the intradermal induction exposure (2 animals):
- Concentration: 10 and 25%; and 2 and 5%
- Amounts: 0.1 mL. Each of the 2 animals received 2 different concentrations in the right and left clipped shoulder regions.
- Scoring: the skin reactions were scored 24 and 48 hours after application
For the epicutaneous induction, using Scotchpak-non-woven patch (the same animals as above):
- Concentration: 50 and 25%
- Amount: 0.5 mL. Each of the 2 animals received a differerent concentration to the shaved flank of the animal.
- Exposure period: 24 hours (occlusive)
- Scoring: the skin reactions were scored 24 and 48 hours after patch removal
For the epicutaneous induction, using square chambers (2 animals):
- Concentration: 50, 25, 10 and 5%
- Amount: 0.05 mL were applied occlusively on a shaved flank of each of the 2 animals.
- Exposure period: 24 hours (occlusive)
- Scoring: the skin reactions were scored 24 and 48 hours after patch removal
MAIN STUDY
Test animals: 10
Control animals: 5
A. INDUCTION EXPOSURE
- No. of exposures: 2
1) Intradermal injections on day 1:
- Concentration: 25%
- Site: clipped scapular region. One of each pair was on each side of the midline and from cranial A) to caudal C):
Three pairs of intradermal injections:
1) 0.1 mL: FCA (50% in water)
2) 0.1 mL: test substance at a 25% concentration in distilled water (control animals: 0.1 mL distilled water)
3) 0.1 mL: 50% test substance in distilled water + 50% FCA (undiluted) (control animals: 50% with distilled water + 50% FCA (undiluted))
-Readings: on day 3 (48 hrs after the injections). Irritating results were observed in the test groups, in each of the 3 sites.
- Use of SDS (all animals): on day 7, 24 hrs before the topical induction application, the scapular area was clipped and subsequently rubbed with 10% SDS in vaseline using a spatula.
2)Topical application on day 8:
- Concentration: 50%
- Amount: 0.5 mL (control animals: 0.5 mL of distilled water), on the SDS treated area
- Exposure period: 48 hours (occlusive)
- Readings: scores were rated directly after patch removal (skin cleaned of residual test substance)
B. CHALLENGE EXPOSURE (all animals)
- Concentration: 0 and 50%
- Day of challenge: day 22 (13 days after the start of the 2nd induction)
- Exposure period: 24 hours (occlusive)
- Site: flank
- Amount: 0.5 mL
- Readings: scores were rated 24 and 48 hours after patch removal - Challenge controls:
- Not applicable.
- Positive control substance(s):
- yes
- Remarks:
- (the results of the latest reliability check, performed in May 1996 with Alpha-hexylcinnamicaldehyde, tech. 85%, are reported)
- Positive control results:
- The latest reliability check (performed less than 6 months ago) shows a sensitisation rate of 100%. See the attached background material.
- Reading:
- 1st reading
- Hours after challenge:
- 24
- Group:
- test chemical
- Dose level:
- 50 %
- No. with + reactions:
- 0
- Total no. in group:
- 10
- Remarks on result:
- other: Reading: 1st reading. . Hours after challenge: 24.0. Group: test group. Dose level: 50 %. No with. + reactions: 0.0. Total no. in groups: 10.0.
- Reading:
- 2nd reading
- Hours after challenge:
- 48
- Group:
- test chemical
- Dose level:
- 50 %
- No. with + reactions:
- 0
- Total no. in group:
- 10
- Remarks on result:
- other: Reading: 2nd reading. . Hours after challenge: 48.0. Group: test group. Dose level: 50 %. No with. + reactions: 0.0. Total no. in groups: 10.0.
- Reading:
- 1st reading
- Hours after challenge:
- 24
- Group:
- negative control
- Dose level:
- 50 %
- No. with + reactions:
- 0
- Total no. in group:
- 5
- Remarks on result:
- other: Reading: 1st reading. . Hours after challenge: 24.0. Group: negative control. Dose level: 50 %. No with. + reactions: 0.0. Total no. in groups: 5.0.
- Reading:
- 2nd reading
- Hours after challenge:
- 48
- Group:
- negative control
- Dose level:
- 50 %
- No. with + reactions:
- 0
- Total no. in group:
- 5
- Remarks on result:
- other: Reading: 2nd reading. . Hours after challenge: 48.0. Group: negative control. Dose level: 50 %. No with. + reactions: 0.0. Total no. in groups: 5.0.
- Reading:
- 1st reading
- Hours after challenge:
- 24
- Group:
- positive control
- Dose level:
- 50%
- No. with + reactions:
- 10
- Total no. in group:
- 10
- Remarks on result:
- positive indication of skin sensitisation
- Reading:
- 2nd reading
- Hours after challenge:
- 48
- Group:
- positive control
- Dose level:
- 50%
- No. with + reactions:
- 10
- Total no. in group:
- 10
- Remarks on result:
- positive indication of skin sensitisation
- Interpretation of results:
- other: Not sensitising.
- Remarks:
- According Regulation (EC) No. 1272/2008 and its amendments.
- Conclusions:
- In an adjuvant type guinea pig test method for skin sensitisation according to OECD 406 guideline and GLP principles, none of the ten experimental animals showed positive reactions during challenge with Alcamizer 5.
- Executive summary:
Alcamizer 5 was tested in an adjuvant type guinea pig test method for skin sensitisation according to OECD 406 guideline and GLP principles.
After intradermal injection (sites without FCA): On day 3 slight/well defined erythema was observed in all animals (experimental).
Control animals showed no reactions.
On day 10, one animal showed eschar formation and 6 from the 10 animals showed slight/well-defined erythema. All control animals showed slight erythema, except for one animal who showed severy erythema with eschar formation. The reactions noted in the experimental and control animals were considered to be enhanced by the SDS treatment. After the challenge, no skin reactions were evident after the challenge exposure. None of the ten experimental animals showed positive reactions during challenge with Alcamizer 5 48 hours after patch removal.
The latest reliability check (performed less than 6 months ago) shows a sensitisation rate of 100%.
- Endpoint:
- skin sensitisation: in vitro
- Data waiving:
- study scientifically not necessary / other information available
- Justification for data waiving:
- an in vitro skin sensitisation study does not need to be conducted because adequate data from an in vivo skin sensitisation study are available
Referenceopen allclose all
- In the pre-liminary test, discrete or patchy erythema observed at intradermal induction with 25% test substance in the animal. Therefore 25% for the intradermal induction was used.
- Maximum concentration not causing irritating effects in the preliminary epidermal test was 50 %.
Main test:
Signs of irritation after induction:
After intradermal injection (sites without FCA):
On day 3 moderate/severe erythema with or without necrosis
was observed in all animals (experimental). On day 11, 9/10
animals showed eschar formation and 10/10 animals showed
moderate/severe erythema. Control animals showed no reactions.
Signs after epidermal application:
9/10 experimental animals showed very slight to severe
erythema. 2/10 animals also showed eschar/crust formation.
1/5 control animals showed very slight erythema.
Challenge:
No skin reactions were evident after the challenge exposure.
Two animals showed discrete or patchy erythema in repsonse to the 50, 25 and 10% test substance concentrations 48 hours after patch removal. One other animal showed scaliness is response to the 50% concentration.
Two of the ten experimental animals were considered indicative of sensitisation.
One control animal died by accident on day 22. Pink discolouration of the lungs was found at post mortem macroscopic examination of this animal.
No further mortality occurred and no symptoms of systemic toxicity were observed in the animals of the main study during the study period.
The average body weight of the experimental animals and the control animals was within an acceptable range at the beginning and the end of the study.
- In the pre-liminary test, discrete or patchy erythema observed at intradermal induction with 25% test substance in the animal. Therefore 25% for the intradermal induction was used.
- Maximum concentration not causing irritating effects in the preliminary epidermal test was 50 %.
Main test:
Signs of irritation during induction:
After intradermal injection (sites without FCA): On day 3 slight/well defined erythema was observed in all animals (experimental).
Control animals showed no reactions.
On day 10, one animal showed eschar formation and 6 from the 10 animals showed slight/well-defined erythema. All control animals showed slight erythema, except for one animal who showed severy erythema with eschar formation. The reactions noted in the experimental and control animals were considered to be enhanced by the SDS treatment.
Challenge:
No skin reactions were evident after the challenge exposure.
No mortality occurred and no symptoms of systemic toxicity were observed in the animals of the main study during the study period.
Body weight and body weight gain of the experimental animals remained in the same range as controls over the study period.
Endpoint conclusion
- Endpoint conclusion:
- no adverse effect observed (not sensitising)
- Additional information:
First study:
Alcamizer 5 was tested in an adjuvant type guinea pig test method for skin sensitisation according to OECD 406 guideline and GLP principles.
After intradermal injection (sites without FCA) on day 3, moderate/severe erythema with or without necrosis was observed in all animals (experimental). On day 11, nine of the ten animals showed eschar formation and all ten animals showed moderate/severe erythema. Control animals showed no reactions. After epidermal application, nine of the ten experimental animals showed very slight to severe erythema. Two of the ten animals also showed eschar/crust formation. One of the five control animals showed very slight erythema.
One control animal died by accident on day 22. Pink discolouration of the lungs was found at post mortem macroscopic examination of this animal. No further mortality occurred and no symptoms of systemic toxicity were observed in the animals of the main study during the study period.
After the challenge, no skin reactions were evident after the challenge exposure.
Two animals showed discrete or patchy erythema in repsonse to the 50, 25 and 10% test substance concentrations 48 hours after patch removal. One other animal showed scaliness is response to the 50% concentration. These results lead to a sensitisation rate of 20%. The latest reliability check shows a sensitisation rate of 90%.
Second study:
Alcamizer 5 was tested in an adjuvant type guinea pig test method for skin sensitisation according to OECD 406 guideline and GLP principles.
After intradermal injection (sites without FCA): On day 3 slight/well defined erythema was observed in all animals (experimental).
Control animals showed no reactions.
On day 10, one animal showed eschar formation and 6 from the 10 animals showed slight/well-defined erythema. All control animals showed slight erythema, except for one animal who showed severy erythema with eschar formation. The reactions noted in the experimental and control animals were considered to be enhanced by the SDS treatment. After the challenge, no skin reactions were evident after the challenge exposure. None of the ten experimental animals showed positive reactions during challenge with Alcamizer 5 48 hours after patch removal.
The latest reliability check shows a sensitisation rate of 100%.
Respiratory sensitisation
Endpoint conclusion
- Endpoint conclusion:
- no study available
Justification for classification or non-classification
Based on the study results, Alcamizer 5 does not have to be classified and has no obligatory labelling requirement for skin sensitisation according to Regulation (EC) No 1272/2008 on classification, labelling and packaging of substances and mixtures (including all amendments).
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