Registration Dossier

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Please be aware that this old REACH registration data factsheet is no longer maintained; it remains frozen as of 19th May 2023.

The new ECHA CHEM database has been released by ECHA, and it now contains all REACH registration data. There are more details on the transition of ECHA's published data to ECHA CHEM here.

Diss Factsheets

Administrative data

Endpoint:
melting point/freezing point
Type of information:
experimental study
Adequacy of study:
key study
Reliability:
2 (reliable with restrictions)
Rationale for reliability incl. deficiencies:
other: This study was selected as the key study because the information provided for the hazard endpoint is sufficient for the purpose of classification and labelling and/or risk assessment.

Data source

Reference
Reference Type:
study report
Title:
Unnamed
Year:
2013
Report date:
2013

Materials and methods

Principles of method if other than guideline:
Melting point determination was performed on a Buchi B-545 melting point apparatus with photocell detection.
GLP compliance:
no
Type of method:
capillary method

Test material

Constituent 1
Chemical structure
Reference substance name:
2-amino-3-hydroxy-N'-[(E)-(2,3,4-trihydroxyphenyl)methylidene]propanehydrazide hydrochloride
EC Number:
940-411-0
Cas Number:
1353749-74-2
Molecular formula:
C10H14ClN3O5
IUPAC Name:
2-amino-3-hydroxy-N'-[(E)-(2,3,4-trihydroxyphenyl)methylidene]propanehydrazide hydrochloride
Details on test material:
- Purity: 99.9%

Results and discussion

Melting / freezing point
Melting / freezing pt.:
218 °C
Decomposition:
no
Remarks on result:
other: range 218.0 - 218.6 ± 0.6°C

Any other information on results incl. tables

EVALUATION: The three samples gave a melting point of 218°C, with the range 218.0 - 218.6 ± 0.6°C.

Applicant's summary and conclusion

Conclusions:
This study and the conclusions which are drawn from it fulfil the quality criteria (validity, reliability, repeatability).
Melting point of 218°C
Executive summary:

Three replicate samples of test substance were prepared in three different capillaries and measurements were made.

The three samples gave a melting point of 218°C, with the range 218.0 - 218.6 ± 0.6°C.