Registration Dossier

Data platform availability banner - registered substances factsheets

Please be aware that this old REACH registration data factsheet is no longer maintained; it remains frozen as of 19th May 2023.

The new ECHA CHEM database has been released by ECHA, and it now contains all REACH registration data. There are more details on the transition of ECHA's published data to ECHA CHEM here.

Diss Factsheets

Physical & Chemical properties

Melting point / freezing point

Currently viewing:

Administrative data

Link to relevant study record(s)

Reference
Endpoint:
melting point/freezing point
Type of information:
experimental study
Adequacy of study:
key study
Study period:
01 June 2017 - 20 June 2017
Reliability:
1 (reliable without restriction)
Rationale for reliability incl. deficiencies:
guideline study
Qualifier:
according to guideline
Guideline:
OECD Guideline 102 (Melting point / Melting Range)
Version / remarks:
27 July 1995
Deviations:
no
Qualifier:
according to guideline
Guideline:
EPA OPPTS 830.7200 (Melting Point / Melting Range)
Version / remarks:
March 1998
Deviations:
no
Qualifier:
according to guideline
Guideline:
EU Method A.1 (Melting / Freezing Temperature)
Version / remarks:
May 2008
Deviations:
no
Qualifier:
according to guideline
Guideline:
other: CIPAC Handbook Volume F, Physico-chemical Methods for Technical and Formulated Pesticides, MT 139 Pour Point of Mineral Oil
Deviations:
no
GLP compliance:
yes (incl. QA statement)
Type of method:
pour point
Key result
Melting / freezing pt.:
39 °C
Atm. press.:
1 013.25 hPa
Decomposition:
no
Sublimation:
no

The test jar was cooled from 44.6 and 44.9 °C and examined at intervals of 3 °C for flow characteristics.

Table 1: Experiment 1- Determination of the Pour Point of the test item

 Temperature [°C]  Observation
 44.6  moved
 41.6  moved
 38.6  moved
 35.6  did not move

Table 2: Experiment 2- Determination of the Pour Point of the test item

 Temperature [°C]  Observation
 44.9  moved
 41.9  moved
 38.9  moved
 35.9  did not move
Conclusions:
The pour point of the test item was determined to be 39 °C at 1013 hPa.
Executive summary:

A study was conducted according to OECD TG 102, EU method A.1 and EPA OPPTS 830.7200 to determine the pour point of the test item. The pour point was determined from the lowest temperature at which movement of the test item was observed in a closed test jar. The determination was performed in duplicate. The pour point of the test item was determined to be 39 °C at 1013 hPa.

Description of key information

The pour point of the test item was determined to be 39 °C at 1013 hPa.

Key value for chemical safety assessment

Melting / freezing point at 101 325 Pa:
39 °C

Additional information

A study was conducted according to OECD TG 102 and EU method A.1 and EPA OPPTS 830.7200 to determined the pour point of the test item. The pour point was determined from the lowest temperature at which movement of the test item was observed in a closed test jar. The determination was performed in duplicate. The pour point of the test item was determined to be 39°C at 1013 hPa.