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Physical & Chemical properties

Melting point / freezing point

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Administrative data

Link to relevant study record(s)

Reference
Endpoint:
melting point/freezing point
Type of information:
experimental study
Adequacy of study:
key study
Study period:
This study was conducted between 21 April 2017 and 03 June 2017
Reliability:
1 (reliable without restriction)
Rationale for reliability incl. deficiencies:
guideline study
Qualifier:
according to guideline
Guideline:
OECD Guideline 102 (Melting point / Melting Range)
Version / remarks:
27 July 1995
Deviations:
no
Qualifier:
according to guideline
Guideline:
EU Method A.1 (Melting / Freezing Temperature)
Version / remarks:
EC No. 440/2008 of 30 May 2008
Deviations:
no
GLP compliance:
yes (incl. QA statement)
Type of method:
pour point
Specific details on test material used for the study:
Information as provided by the Sponsor.
Identification: 2-methylene-1, 3-propanediol diacetate (CAS: 3775-29-9)
Appearance/Physical state: Clear colorless liquid
Batch: 20160308(-88)
Purity: 99.7%
Expiry date: 31 March 2019
Storage conditions: Room temperature in the dark [Stored at approximate 4 °C between 02 September 2016 and 08 February 2017, room temperature after this time]
Key result
Melting / freezing pt.:
< -20 °C
Decomposition:
no

Results

Preliminary Test

The pour point of the preliminary test was less than -20 °C (<253 K).

 Discussion

As the test item did not reach a stationary point during the preliminary analysis a definitive test was not required and a limit value of less than -20 °C (<253 K) was applied.  

Conclusions:
The pour point of the test item has been determined to be less than -20 °C (<253 K).
Executive summary:

The general physico-chemical properties of 2-methylene-1, 3-propanediol diacetate (CAS: 3775-29-9) have been determined.

Melting/Freezing Point Less than -20 °C (253 K) using pour point method, designed to be compatible with Method A.1 Melting/Freezing Temperature of Commission Regulation (EC) No 440/2008 of 30 May 2008 and Method 102 of the OECD Guidelines for Testing of Chemicals, 27 July 1995.

Description of key information

The general physico-chemical properties of 2-methylene-1, 3-propanediol diacetate (CAS: 3775-29-9) have been determined.


Melting/Freezing Point - Less than -20 °C (253 K) using pour point method, designed to be compatible with Method A.1 Melting/Freezing Temperature of Commission Regulation (EC) No 440/2008 of 30 May 2008 and Method 102 of the OECD Guidelines for Testing of Chemicals, 27 July 1995


 

Key value for chemical safety assessment

Melting / freezing point at 101 325 Pa:
-20 °C

Additional information