Registration Dossier
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EC number: 814-345-7 | CAS number: 2003244-43-5
Melting point / freezing point
Administrative data
Link to relevant study record(s)
- Endpoint:
- melting point/freezing point
- Type of information:
- experimental study
- Adequacy of study:
- key study
- Study period:
- The study was conducted between 08 March 2016 and 29 April 2016.
- Reliability:
- 1 (reliable without restriction)
- Rationale for reliability incl. deficiencies:
- guideline study
- Justification for type of information:
- The study is considered to be a reliability 1 as it has been conducted according to OECD Test Guideline 102 using the differential scanning calorimetry method and in compliance with GLP.
- Qualifier:
- according to guideline
- Guideline:
- OECD Guideline 102 (Melting point / Melting Range)
- Version / remarks:
- 27 July 1995
- Deviations:
- no
- GLP compliance:
- yes (incl. QA statement)
- Type of method:
- differential scanning calorimetry
- Specific details on test material used for the study:
- Identification: ES421 Pinyl Nitrile
SOURCE OF TEST MATERIAL
- Appearance/physical state: white solid
- Source and lot/batch No.of test material: SM15077102
- Expiration date of the lot/batch: 22 July 2016
- Purity: 98.08%
STABILITY AND STORAGE CONDITIONS OF TEST MATERIAL
- Storage condition of test material: approximately 4 °C, in the dark - Key result
- Melting / freezing pt.:
- 311 K
- Conclusions:
- The melting point of the test item, ES421 Pinyl Nitrile, has been determined to be 38 °C (311 K).
- Executive summary:
The melting point of the test substance, ES421 Pinyl Nitrile, was 38 °C (311 K) by differential scanning calorimetry, using a proceduredesigned to be compatible with Method A.1 Melting/Freezing Temperature of CommissionRegulation (EC) No 440/2008 of 30 May 2008, and Method 102 of the OECD Guidelines forTesting of Chemicals, 27 July 1995.
Reference
Thermographic data for determinations 1 and 2 are shown in the followingtables:
Determination 1:
Heating Step |
Thermal Event |
Interpretation |
Temperature |
|
°C |
K |
|||
1 |
Endotherm |
Enthalpy relaxation |
~21 |
~294 |
Endotherm onset temperature |
Melting point |
36.35 |
310 |
|
2 |
Baseline deviation |
Glass transition temperature |
~20 |
~293 |
Endotherm onset temperature |
Melting point |
37.98 |
311 |
|
Determination 2:
Heating Step |
Thermal Event |
Interpretation |
Temperature |
|
°C |
K |
|||
1 |
Endotherm |
Enthalpy relaxation |
~21 |
~294 |
Endotherm onset temperature |
Melting point |
39.48 |
313 |
|
2 |
Baseline deviation |
Glass transition temperature |
~20 |
~293 |
Endotherm onset temperature |
Melting point |
39.19 |
312 |
|
Description of key information
The
melting point of the test substance, ES421 Pinyl Nitrile, was 38 °C (311
K) by differential scanning calorimetry, using a proceduredesigned
to be compatible with Method A.1 Melting/Freezing Temperature of
CommissionRegulation
(EC) No 440/2008 of 30 May 2008, and Method 102 of the OECD Guidelines
forTesting
of Chemicals, 27 July 1995.
Key value for chemical safety assessment
- Melting / freezing point at 101 325 Pa:
- 38 °C
Additional information
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